[1,1′-二环戊基]-1,1'-二醇合成路线 （共 38 条）
反应条件
orthoformic acid triethyl ester
1.) 135 deg C, 4 h, 2.) 175 deg C, 3 h; Yield given. Multistep reaction;
参考文献
Kopecky, Karl R.; Sastre, Juan A. Lopez
Canadian Journal of Chemistry, 1980 , vol. 58, # 19 p. 2089 - 2092
反应条件
4-(N,N-dimethlyamino)pyridine
T=85°C; 4 h;
参考文献
Bhushan, Vidya; Chakraborty, Thushar K.; Chandrasekaran, Srinivasan
Journal of Organic Chemistry, 1984 , vol. 49, # 21 p. 3974 - 3978
反应条件
chlorosulphonyl isocyanate in benzene
1.) 0 deg C, 2.) reflux, 0.5 h;
参考文献
Joseph, Sajan P.; Dhar, D. N.
Synthetic Communications, 1988 , vol. 18, # 18 p. 2295 - 2302
反应条件
in benzene
1.) 0 deg C, 2.) reflux, 0.5 h;
参考文献
Joseph, Sajan P.; Dhar, D. N.
Synthetic Communications, 1988 , vol. 18, # 18 p. 2295 - 2302
反应条件
iron (III) acetylacetonate in various solvent(s)
2.5 h; Ambient temperature;
参考文献
Hamann, Beatrice; Namy, Jean-Louis; Kagan, Henri B.
Tetrahedron, 1996 , vol. 52, # 45 p. 14225 - 14234
反应条件
1: cerium; Monobrombernsteinsaeuraethylester (germ.)=monobromo ethyl succinate With iodine in tetrahydrofuran
T=0°C; 0.5 h; Inert atmosphere;
2: cyclopentanone in tetrahydrofuran
T=0 - 20°C; 3.5 h; Inert atmosphere;
参考文献
Rodrigues, Shirley M. M.; Nardini, Viviani; Constantino, Mauricio G.; Da Silva, Gil Valdo J.
Tetrahedron Letters, 2012 , vol. 53, # 45 p. 6136 - 6137,2
反应条件
cerium in tetrahydrofuran
2 h; Ambient temperature;
参考文献
Fukuzawa, Shin-ichi; Fujinami, Tatsuo; Sakai, Shizuyoshi
Journal of the Chemical Society, Chemical Communications, 1986 , # 6 p. 475 - 476
反应条件
Ti(OiPr)4 in diethyl ether
15 h;
参考文献
Matiushenkov, Evgenii A.; Sokolov, Nikolai A.; Kulinkovich, Oleg G.
Synlett, 2004 , # 1 p. 77 - 80
反应条件
N,N,N',N',N'',N''-hexamethylphosphoric triamide; samarium diiodide in tetrahydrofuran
Ambient temperature;
参考文献
Csuk; Hu; Abdou; Kratky
Tetrahedron, 1991 , vol. 47, # 34 p. 7037 - 7044
反应条件
titanium tetrachloride in tetrahydrofuran
1.5 h;
参考文献
Fuerstner, Alois; Csuk, Rene; Rohrer, Christian; Weidmann, Hans
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1988 , p. 1729 - 1734
