1,1-环丁烷二羰基二氯化物合成路线 （共 9 条）
反应条件
1: SO2Cl2, (PhCO)2O2 / 3 h / Heating 2: H2O 3: 12 h / 180 °C 4: (i) Et2O, (ii) LiAlH4 5: KOtBu / dimethylsulfoxide 6: H2 / PtO2 / methanol View Scheme
参考文献
Hanack,M.; Riedlinger,K.
Chemische Berichte, 1967 , vol. 100, p. 2107 - 2116
反应条件
1: SO2Cl2, (PhCO)2O2 / 3 h / Heating 2: H2O 3: 12 h / 180 °C View Scheme
参考文献
Hanack,M.; Riedlinger,K.
Chemische Berichte, 1967 , vol. 100, p. 2107 - 2116
反应条件
1: SO2Cl2, (PhCO)2O2 / 3 h / Heating 2: H2O 3: 12 h / 180 °C 4: (i) Et2O, (ii) LiAlH4 5: KOtBu / dimethylsulfoxide View Scheme
参考文献
Hanack,M.; Riedlinger,K.
Chemische Berichte, 1967 , vol. 100, p. 2107 - 2116
反应条件
1: SO2Cl2, (PhCO)2O2 / 3 h / Heating 2: H2O 3: 12 h / 180 °C 4: diethyl ether View Scheme
参考文献
Hanack,M.; Riedlinger,K.
Chemische Berichte, 1967 , vol. 100, p. 2107 - 2116
反应条件
1: SO2Cl2, (PhCO)2O2 / 3 h / Heating 2: H2O 3: 12 h / 180 °C 4: (i) Et2O, (ii) LiAlH4 View Scheme
参考文献
Hanack,M.; Riedlinger,K.
Chemische Berichte, 1967 , vol. 100, p. 2107 - 2116
反应条件
sulfuryl dichloride; dibenzoyl peroxide
3 h; Heating;
参考文献
UNIVERSITAeT REGENSBURG
Patent: WO2004/99224 A1, 2004 ;
Location in patent: Page/Page column 9-10 ;
反应条件
sulfuryl dichloride; meta-chloroperoxybenzoic acid in benzene
8 h; Heating; Title compound not separated from byproducts;
参考文献
Prelog, Vladimir; Thix, Jean; Srikrishnan, Tamarapu
Helvetica Chimica Acta, 1982 , vol. 65, # 8 p. 2622 - 2644
反应条件
1: SO2Cl2, (PhCO)2O2 / 3 h / Heating
2: H2O
View Scheme
参考文献
Hanack,M.; Riedlinger,K.
Chemische Berichte, 1967 , vol. 100, p. 2107 - 2116
反应条件
thionyl chloride
3 h; Heating;
参考文献
Hanack,M.; Riedlinger,K.
Chemische Berichte, 1967 , vol. 100, p. 2107 - 2116
