1,4-二碘-2-(三氟甲基)苯合成路线 （共 2 条）
反应条件
N,N,N',N',N'',N''-hexamethylphosphoric triamide; copper(l) iodide; potassium iodide
T=145°C; 19 h;
参考文献
Ikegami, Hideo; Chong, Chin-Hong; Yamochi, Hideki; Saito, Gunzi
Molecular Crystals and Liquid Crystals Science and Technology Section A: Molecular Crystals and Liquid Crystals, 2002 , vol. 382, p. 21 - 35
反应条件
1.1: 95 percent / BF3*Et2O; t-BuONO / tetrahydrofuran / 0.5 h / -20 - 5 °C
2.1: propylaminomethyl polystyrene; K2CO3 / tetrahydrofuran; dimethylformamide / 1.08 h / 0 - 20 °C
2.2: 37 mg / CH3I / acetonitrile / 24 h / 110 °C
View Scheme
参考文献
Hwang, Jiunn-Jye; Tour, James M.
Tetrahedron, 2002 , vol. 58, # 52 p. 10387 - 10405
