1,2,3,4-四氢萘-2-甲腈合成路线 （共 14 条）
反应条件
nickel in ethylene glycol dimethyl ether
Ambient temperature;
参考文献
Inaba, Shin-ichi; Wehmeyer, Richard M.; Forkner, Matthew W.; Rieke, Reuben D.
Journal of Organic Chemistry, 1988 , vol. 53, # 2 p. 339 - 344
反应条件
chromium dichloride in tetrahydrofuran; N,N,N',N',N'',N''-hexamethylphosphoric triamide
参考文献
Stephan, D.; Gorgues, A.; le Coq, A.
Tetrahedron Letters, 1984 , vol. 25, # 49 p. 5649 - 5652
反应条件
tetra(tert-butyl)-ammonium fluoride in acetonitrile
1 h; Ambient temperature;
参考文献
Ito; Nakatsuka; Saegusa
Journal of the American Chemical Society, 1982 , vol. 104, # 26 p. 7609 - 7622
反应条件
DPPE-Pd(η3-C3H5)Cp in dimethyl sulfoxide
T=140°C; 72 h;
参考文献
Kuwano, Ryoichi; Shige, Takenori
Journal of the American Chemical Society, 2007 , vol. 129, # 13 p. 3802 - 3803
反应条件
tetrabutyl ammonium fluoride in dichloromethane
1.5 h; Ambient temperature;
参考文献
Ito,Y.; Nakatsuka,M.; Saegusa,T.
Journal of the American Chemical Society, 1980 , vol. 102, p. 863
反应条件
1: With resin-bound amine; benzotriazol-1-ol; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate in N,N-dimethyl-formamide
T=20°C;
2: With pyridine; trifluoroacetic anhydride in dichloromethane
T=20°C; 16 h;
参考文献
Hone, Neal D.; Payne, Lloyd J.; Tice, Colin M.
Tetrahedron Letters, 2001 , vol. 42, # 6 p. 1115 - 1118
反应条件
1: 99 percent / pyridine / CH2Cl2 / 0 - 20 °C
2: 42 percent / DPPE-Pd(η3-C3H5)Cp / dimethylsulfoxide / 72 h / 140 °C
View Scheme
参考文献
Kuwano, Ryoichi; Shige, Takenori
Journal of the American Chemical Society, 2007 , vol. 129, # 13 p. 3802 - 3803
反应条件
potassium fluoride in N,N-dimethyl-formamide
T=100°C; 3 h;
参考文献
Kuwano, Ryoichi; Shige, Takenori
Chemistry Letters, 2005 , vol. 34, # 5 p. 728 - 729
反应条件
cesium fluoride in N,N-dimethyl-formamide
24 h; Ambient temperature;
参考文献
Maeda, Yasuhiro; Sato, Yoshiro
Journal of Organic Chemistry, 1996 , vol. 61, # 15 p. 5188 - 5190
反应条件
fluoride in acetonitrile
Elimination; Diels-Alder reaction;
参考文献
Di Valentin, Cristiana; Freccero, Mauro; Sarzi-Amade, Mirko; Zanaletti, Riccardo
Tetrahedron, 2000 , vol. 56, # 16 p. 2547 - 2559
