(乙氧基羰基甲基)二甲基溴化硫鎓合成路线 （共 32 条）
反应条件
(i) BH3, (ii) /BRN= 4161472/, NaH, (iii) aq. H2O2, NaOH; Multistep reaction;
参考文献
Tufariello,J.J. et al.
Journal of the American Chemical Society, 1967 , vol. 89, # 25 p. 6804 - 6805
反应条件
potassium hydroxide; N-benzyl-N,N,N-triethylammonium chloride in tetrahydrofuran T=20°C; 4 h;
参考文献
Galin, F. Z.; Iskandarova, V. N.; Tolstikov, G. A.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1988 , vol. 37, p. 708 - 712
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1988 , # 4 p. 828 - 833
反应条件
1: (Ethoxycarbonylmethyl)dimethyl-sulfonium bromide With caesium carbonate in anhydrous xylene T=20°C; 2: C14H13BrClNO2S in anhydrous xylene T=20°C; 3: With potassium tert-butylate in anhydrous xylene T=20°C; 72 h;
参考文献
Yang, Qing-Qing; Xiao, Cong; Lu, Liang-Qiu; An, Jing; Tan, Fen; Li, Bin-Jie; Xiao, Wen-Jing
Angewandte Chemie - International Edition, 2012 , vol. 51, # 36 p. 9137 - 9140
反应条件
sodium ethanolate 1.) ethanol; 2.) warming; Yield given. Multistep reaction;
参考文献
Canadian Journal of Chemistry, , vol. 62, # 8 p. 1580 - 1584
反应条件
potassium carbonate; N,N,N',N'-tetramethylguanidine in water; acetonitrile T=23°C;
参考文献
Tetrahedron Letters, , vol. 48, # 18 p. 3277 - 3279
反应条件
(i) BH3, (ii) /BRN= 4161472/, NaH, (iii) aq. H2O2, NaOH; Multistep reaction;
参考文献
Tufariello,J.J. et al.
Journal of the American Chemical Society, 1967 , vol. 89, # 25 p. 6804 - 6805
反应条件
1,8-diazabicyclo[5.4.0]undec-7-ene in acetonitrile
T=20°C;
参考文献
ELI LILLY AND COMPANY
Patent: WO2003/104217 A2, 2003 ;
Location in patent: Page 96 ;
反应条件
Yield given. Multistep reaction;
参考文献
Deng, Min-Zhi; Li, Nan-Sheng; Huang, Yao-Zeng
Journal of Organic Chemistry, 1992 , vol. 57, # 14 p. 4017 - 4019
反应条件
Yield given. Multistep reaction;
参考文献
Deng, Min-Zhi; Li, Nan-Sheng; Huang, Yao-Zeng
Journal of Organic Chemistry, 1992 , vol. 57, # 14 p. 4017 - 4019
反应条件
sodium ethanolate
1.) ethanol; 2.) warming; Yield given. Multistep reaction;
参考文献
McKinnon; Duncan; Millar
Canadian Journal of Chemistry, 1984 , vol. 62, # 8 p. 1580 - 1584
