反应条件
1: 70 percent / 1,3-diaminopropane, sodamide / 2 h / 80 °C
2: 83 percent / pyridine / 24 h / 10 °C
3: 80 percent / NaI / butan-2-one / 18 h / Heating
4: 1.) catecholborane, 2.) NaI, chloramine-T / 1.) 55 deg C, 6 h, 2.) THF, water, 0 deg C, 15 min
View Scheme
参考文献
Knapp, F.F.; Srivastava, P.C.; Callahan, A.P.; Cunningham, E.B.; Kabalka, G.W.; Sastry, K.A.R.
Journal of Medicinal Chemistry, 1984 , vol. 27, # 1 p. 57 - 63
