反应条件
in dichloromethane
soln. of perchlorate added to soln. of Fe-compound (room temp., with stirring), mixt. stirred 60min, addn. of ether, mixt. allowed to stand (2d, 7-8°C), crystn.; ppt. filtered, washed with ether, dried over P2O5; elem. anal.;
参考文献
Boev, V. I.
Journal of General Chemistry USSR (English Translation), 1990 , vol. 60, p. 1833 - 1837
Zhurnal Obshchei Khimii, 1990 , vol. 60, p. 2054 - 2059