lithium aluminium tetrahydride in diethyl ether
1.) 0 deg C up to RT; 2.) RT, 1 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Plack, Volker; Muenchenberg, Jochen; Thoennessen, Holger; Jones, Peter G.; Schmutzler, Reinhard
European Journal of Inorganic Chemistry, 1998 , # 6 p. 865 - 875
Chadwick, Derek J.; Hodgson, Simon T.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , # 1 p. 93 - 102
Chadwick, Derek J.; Hodgson, Simon T.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , # 1 p. 93 - 102
in dichloromethane
To a soln. of complex in CH2Cl2 was added dropwise with stirring a soln. of CPh3BF4 in CH2Cl2 at room temp. (inert atm.);; filtered,;
参考文献
Barabotti, Paolo; Diversi, Pietro; Ingrosso, Giovanni; Lucherini, Antonio; Nuti, Franca
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1984 , p. 2517 - 2524
