sodium methylate; nitrobenzene in various solvent(s)
8 h; Heating; Further byproducts given;
参考文献
Huszthy, Peter; Lempert, Karoly; Simig, Gyula
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1985 , p. 1323 - 1330
sodium methylate in various solvent(s)
10 h; Heating; Further byproducts given;
参考文献
Huszthy, Peter; Lempert, Karoly; Simig, Gyula
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1985 , p. 1323 - 1330
→
反应条件
sulfuric acid in ethanol
10 h; Heating;
参考文献
Bella, A. Franco; Slawin, Alexandra M. Z.; Walton, John C.
Journal of Organic Chemistry, 2004 , vol. 69, # 18 p. 5926 - 5933
1: oxalyl chloride, pyridine / benzene / 4 h / Heating
2: 6.5 g / sodium azide / dioxane; H2O / Ambient temperature
3: toluene / 3 h / Heating
4: 80 percent / 3 h / Heating
5: 1.) sodium, liquid ammonia, 2.) pyridine / 1.) methanol, 2.) CH2Cl2, 0 deg C, 2 h
View Scheme
参考文献
Chadwick, Derek J.; Hodgson, Simon T.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , # 1 p. 93 - 102
