反应条件
in tetrahydrofuran N2 atmosphere, mixing of solns. of FeCl2*1.5 THF and LiC5H2(SiMe3)3 (-95°C, during 30 min), addn. of C5Me5Li, warming to room temp., stirring (16 h); evapn. to dryness, extraction (pentane), chromy. (Al2O3, pentane), recrystn. of (C5Me5)Fe(C5H2(SiMe3)3) (acetonitrile); elem. anal.;
参考文献
Chemische Berichte, , vol. 121, p. 1899 - 1906
