N,N,N',N,-tetramethylethylenediamine; mono(bis(di-tert-butyl(4-(dimethylamino)phenyl)phosphonio)palladium(II))dichloride; zinc in water T=20°C; 8 h; Inert atmosphere;
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Duplais, Christophe; Krasovskiy, Arkady; Wattenberg, Alina; Lipshutz, Bruce H.
Chemical Communications, 2010 , vol. 46, # 4 p. 562 - 564
1: 4-iodobenzoic acid ethyl ester With isopropylmagnesium chloride in tetrahydrofuran T=-20°C; 2: 4-ethoxycarbonylbenzoyl cyanide With iron (III) acetylacetonate in tetrahydrofuran T=-10°C;
参考文献
Duplais, Christophe; Bures, Filip; Sapountzis, Ioannis; Korn, Tobias J.; Cahiez, Gerard; Knochel, Paul
Angewandte Chemie - International Edition, 2004 , vol. 43, # 22 p. 2968 - 2970