1: benzylamine With n-butyllithium in tetrahydrofuran; hexane
2: N-methyl-N-methoxycrotonamide in tetrahydrofuran; hexane
T=-78 - -70°C; Michael addition; 1.66667 h; diastereoselective reaction;
参考文献
Ma, Li-Jian; Mei, Zhen-Wu; Toyohara, Keisuke; Kawafuchi, Hiroyuki; Nokami, Junzo; Inokuchi, Tsutomu
Bulletin of the Chemical Society of Japan, 2010 , vol. 83, # 12 p. 1545 - 1547
1: benzylamine With n-butyllithium in tetrahydrofuran; hexane
2: tert.-Butyl-percrotonat in tetrahydrofuran; hexane
T=-78 - -70°C; Michael addition; 1.66667 h; diastereoselective reaction;
参考文献
Ma, Li-Jian; Mei, Zhen-Wu; Toyohara, Keisuke; Kawafuchi, Hiroyuki; Nokami, Junzo; Inokuchi, Tsutomu
Bulletin of the Chemical Society of Japan, 2010 , vol. 83, # 12 p. 1545 - 1547