2-氯乙氧基-2-乙氧基二乙醇合成路线 （共 57 条）
反应条件
sodium carbonate T=110°C; 36 h;
参考文献
Maeda, Hirokazu; Furuyoshi, Shigeo; Nakatsuji, Yohji; Okahara, Mitsuo
Tetrahedron, 1982 , vol. 38, # 22 p. 3359 - 3362
反应条件
1: 68 percent / dimethylformamide / 5 h / 120 °C 2: 70 percent / hydrazine hydrate / ethanol / 3 h / Heating 3: 55 percent / Na2CO3 / 36 h / 110 °C View Scheme
参考文献
Iqbal, Mudassir; Huskens, Jurriaan; Sypula, Michal; Modolo, Giuseppe; Verboom, Willem
New Journal of Chemistry, 2011 , vol. 35, # 11 p. 2591 - 2600
反应条件
Yield given. Multistep reaction;
参考文献
Keana, John F. W.; Wu, Yexin; Wu, Guanli
Journal of Organic Chemistry, 1987 , vol. 52, # 12 p. 2571 - 2576
反应条件
in toluene T=40°C; 48 h;
参考文献
Rattay; Rettig
Pharmazie, 1997 , vol. 52, # 9 p. 676 - 679
反应条件
1: With potassium phtalimide in N,N-dimethyl-formamide T=100°C; 19 h; 2: With hydrazine hydrate in ethanol; water 3 h; Reflux;
参考文献
Isono, Takuya; Satoh, Toshifumi; Kakuchi, Toyoji
Journal of Polymer Science, Part A: Polymer Chemistry, 2011 , vol. 49, # 14 p. 3184 - 3192
反应条件
1: hydrogenchloride / 20 °C 2: sodium hydride / tetrahydrofuran / Reflux 3: hydrogenchloride / methanol; dichloromethane / Reflux View Scheme
参考文献
Kawakami, Kazumitsu; Sei, Yoshihisa; Yamaguchi, Kentaro; Tsuda, Akihiko
Journal of Organic Chemistry, 2011 , vol. 76, # 3 p. 875 - 881
反应条件
1: 58.3 g / sodium iodide / butan-2-one / 19 h / Heating 2: 16.7 g / dimethylformamide / 18 h / 95 °C 3: 1.1 g / Jones reagent / acetone / 0.5 h 4: 1.) hydrazine hydrate; 2.) cc. hydrochloric acid / 1.) methanol, reflux, 3 h; 2.) water View Scheme
参考文献
Slama, James; Rando, Robert R.
Carbohydrate Research, 1981 , vol. 88, p. 213 - 222
反应条件
1: pyridine / CH2Cl2 2: 64 percent / NH4Cl / dimethylsulfoxide / 16 h / 70 °C View Scheme
参考文献
Holmes, Brian T.; Snow, Arthur W.
Tetrahedron Letters, 2007 , vol. 48, # 28 p. 4813 - 4815
反应条件
1: N,N-dimethyl-formamide / Inert atmosphere 2: hydrazine / ethanol / Inert atmosphere 3: sodium hydrogencarbonate / water / Inert atmosphere 4: sodium hypochlorite; 2,2,6,6-tetramethyl-piperidine-N-oxyl / dichloromethane / Inert atmosphere View Scheme
参考文献
Journal of the American Chemical Society, , vol. 133, # 32 p. 12382 - 12385
反应条件
chlorine in dichloromethane T=10 - 20°C; 0.25 h; Yield given. Title compound not separated from byproducts;
参考文献
Beger, J.; Poeschmann, C.; Shabanov, A. L.; Gurbanov, P. A.
Journal fuer Praktische Chemie (Leipzig), 1987 , vol. 329, # 6 p. 996 - 1007
