2-氯乙氧基-2-乙氧基二乙醇合成路线 （共 57 条）
反应条件
potassium carbonate; sodium iodide in N,N-dimethyl-formamide
T=80 - 85°C; 35 h;
参考文献
Lukyanenko, Nikolay G.; Kirichenko, Tatiana I.; Lyapunov, Alexander Yu; Mazepa, Alexander V.; Simonov, Yurii A.; Fonari, Marina S.; Botoshansky, Mark M.
Chemistry - A European Journal, 2005 , vol. 11, # 1 p. 262 - 270
反应条件
sodium iodide in acetone
4 h; Heating;
参考文献
Koizumi, Masatoshi; Dietrich-Buchecker, Christiane; Sauvage, Jean-Pierre
European Journal of Organic Chemistry, 2004 , # 4 p. 770 - 775
反应条件
1: 92 percent / NaI / acetone / Heating
2: 95 percent / K2CO3 / acetone / 72 h / Ambient temperature
3: 60 percent / KOH / tetrahydrofuran; H2O / 2 h / 0 °C
4: 13 percent / KOH / dioxane; ethane-1,2-diol / 120 h / 50 °C
View Scheme
参考文献
Czech, B.; Czech, A.; Bartsch, R. A.
Journal of Heterocyclic Chemistry, 1984 , vol. 21, p. 341 - 343
反应条件
1: N,N-dimethyl-formamide / Inert atmosphere
2: hydrazine / ethanol / Inert atmosphere
3: sodium hydrogencarbonate / water / Inert atmosphere
View Scheme
参考文献
Jalisatgi, Satish S.; Kulkarni, Vikas S.; Tang, Betty; Houston, Zachary H.; Lee, Mark W.; Hawthorne, M. Frederick
Journal of the American Chemical Society, 2011 , vol. 133, # 32 p. 12382 - 12385
反应条件
sodium hydrogensulfide in ethanol
Substitution;
参考文献
Boden, Neville; Bushby, Richard J.; Liu, Quanying; Evans, Stephen D.; Toby; Jenkins; Knowles, Peter F.; Miles, Robert E.
Tetrahedron, 1998 , vol. 54, # 38 p. 11537 - 11548
反应条件
hydrogenchloride; sodium hydroxide; thiourea in deoxygenated H2O; water
参考文献
Hutchison, James E.; Woehrle, Gerd H.; Warner, Marvin G.; Brown, Leif O.
Patent: US2009/99044 A1, 2009 ;
反应条件
1: in water
2 h; Heating;
2: With sodium hydroxide
2 h; Heating;
参考文献
Charvet, Nicolas; Reiss, Peter; Roget, Andre; Dapuis, Alain; Gruenwald, Didier; Carayon, Sophie; Chandezon, Frederic; Livache, Thierry
Journal of Materials Chemistry, 2004 , vol. 14, # 17 p. 2638 - 2642
