2-[2-[2-(2-氯乙氧基)乙氧基]乙氧基]乙醇合成路线 (共 15 条)
反应条件
sodium hydroxide in methanol 2 h; Heating;
参考文献
Sokolowski, Adam
Journal of Physical Chemistry, 1989 , vol. 93, # 25 p. 8223 - 8226
反应条件
sodium carbonate; potassium carbonate; benzenesulfonyl chloride 1) 100 - 107 deg C, 3.5 h, 2) dioxane, 70 deg C, 3 h; Yield given. Multistep reaction;
参考文献
Matsushima, Kenji; Nakatsuji, Yohji; Kawamura, Norio; Okahara, Mitsuo
Journal of Heterocyclic Chemistry, 1986 , vol. 23, p. 255 - 256
反应条件
sodium azide; dimethyl sulfoxide T=60°C; 20 h;
参考文献
Bogdan, Niculina D.; Matache, Mihaela; Meier, Veronika M.; Dobrotae, Cristian; Dumitru, Ioana; Roiban, Gheorghe D.; Funeriu, Daniel P.
Chemistry - A European Journal, 2010 , vol. 16, # 7 p. 2170 - 2180
反应条件
1: 45 percent / triphenylphosphine; diethyl azodicarboxylate / toluene / 2 h / 20 °C 2: 35 percent / K2CO3; KI / acetonitrile / 48 h / Heating View Scheme
参考文献
Tetrahedron, , vol. 60, # 23 p. 5041 - 5048
反应条件
1: 64 percent / Na2CO3 / 24 h / 120 °C 2: 59 percent Spectr. / p-toluenesulphonyl chloride, NaOH / dioxane / 5 h / 60 °C View Scheme
参考文献
Maeda, Hirokazu; Furuyoshi, Shigeo; Nakatsuji, Yohji; Okahara, Mitsuo
Tetrahedron, 1982 , vol. 38, # 22 p. 3359 - 3362
反应条件
potassium hydroxide in butan-1-ol 16 h; Heating; Yield given;
参考文献
Loehr, Hans-Gerd; Voegtle, Fritz
Chemische Berichte, 1985 , vol. 118, # 3 p. 914 - 921
参考文献
Gerhardt,W.; Kucharski,S.
Journal fuer Praktische Chemie (Leipzig), 1977 , vol. 319, p. 705 - 712
反应条件
hydrogenchloride
1 h; Ambient temperature;
参考文献
Aarts, Veronika M. L. J.; Grootenhuis, Peter D. J.; Reinhoudt, David N.; Czech, Anna; Czech, Bronislaw P.; Bartsch, Richard A.
Recueil des Travaux Chimiques des Pays-Bas, 1988 , vol. 107, # 2 p. 94 - 104
反应条件
thionyl chloride in toluene
2 h; Heating;
参考文献
MacMahon; Fong II; Baran; Safonov; Wilson; Schuster
Journal of Organic Chemistry, 2001 , vol. 66, # 16 p. 5449 - 5455
反应条件
pyridine; thionyl chloride in toluene
36 h; Heating;
参考文献
Gibson, Harry W.; Nagvekar, Devdatt S.
Canadian Journal of Chemistry, 1997 , vol. 75, # 10 p. 1375 - 1384