Dehydroespeletone; 1-(5-乙酰基-2-甲氧基苯基)-3-甲基丁-2-烯-1-酮合成路线 （共 5 条）
反应条件
potassium carbonate in acetone
2 h; Reflux;
参考文献
Kurina-Sanz, Marcela; Bisogno, Fabricio R.; Lavandera, Ivan; Orden, Alejandro A.; Gotor, Vicente
Advanced Synthesis and Catalysis, 2009 , vol. 351, # 11-12 p. 1842 - 1848
反应条件
N-bromosuccinmide; 2,2'-azo-bisisobutyronitrile in tetrachloromethane
1.5 h; Heating;
参考文献
Bohlmann, Ferdinand; Vorwerk, Edgar
Chemische Berichte, 1980 , vol. 113, # 1 p. 261 - 266
反应条件
1: 95 percent / K2CO3 / acetone / 12 h / Ambient temperature
2: 36 percent / NBS, azoisobutyronitrile / CCl4 / 1.5 h / Heating
View Scheme
参考文献
Bohlmann, Ferdinand; Vorwerk, Edgar
Chemische Berichte, 1980 , vol. 113, # 1 p. 261 - 266
反应条件
1: 51 percent / AlCl3 / 2.5 h / 140 - 160 °C
2: 95 percent / K2CO3 / acetone / 12 h / Ambient temperature
3: 36 percent / NBS, azoisobutyronitrile / CCl4 / 1.5 h / Heating
View Scheme
参考文献
Bohlmann, Ferdinand; Vorwerk, Edgar
Chemische Berichte, 1980 , vol. 113, # 1 p. 261 - 266
反应条件
1: 94 percent / pyridine / CHCl3 / 2 h / Heating
2: 51 percent / AlCl3 / 2.5 h / 140 - 160 °C
3: 95 percent / K2CO3 / acetone / 12 h / Ambient temperature
4: 36 percent / NBS, azoisobutyronitrile / CCl4 / 1.5 h / Heating
View Scheme
参考文献
Bohlmann, Ferdinand; Vorwerk, Edgar
Chemische Berichte, 1980 , vol. 113, # 1 p. 261 - 266
