反应条件
1: 20 percent / AlCl3 / CS2 / room temperature, 30 min; 60 deg C, 2 h 2: 90 percent / 4 M NaOH / ethanol / 2 h / Heating 3: 1) HBF4, NaNO2, 2) Cu, NaNO2 / 1) H2O, 30 min, 2) H2O, 1 h 4: 75 percent / conc. HCl / methanol / 0.5 h / 120 °C 5: 31 percent / KI / toluene / 100 - 110 °C 6: 60 percent / HF, potassium carbonate, potassium oxalate, kryptofix 222 / dimethylsulfoxide / 0.33 h / 160 °C View Scheme
参考文献
Hashizume, Kazunari; Hashimoto, Naoto; Miyake, Yoshihiro
Bulletin of the Chemical Society of Japan, 1997 , vol. 70, # 3 p. 681 - 687
