5-异硫代氰酰基-2-甲氧基吡啶合成路线 （共 5 条）
反应条件
in dichloromethane
T=0 - 20°C; 3.5 h;
参考文献
PFIZER LIMTED
Patent: WO2006/92731 A1, 2006 ;
Location in patent: Page/Page column 49 ;
WO 2006/092731 A1
反应条件
in 1,4-dioxane; sodium hydroxide; (2S)-N-methyl-1-phenylpropan-2-amine hydrate
参考文献
Ciba-Geigy Corporation
Patent: US4001254 A1, 1977 ;
参考文献
Brown, Alan; Brown, T. Bruce; Calabrese, Andrew; Ellis, Dave; Puhalo, Nicholas; Ralph, Michael; Watson, Lesa
Bioorganic and Medicinal Chemistry Letters, 2010 , vol. 20, # 2 p. 516 - 520
反应条件
sodium hydrogencarbonate
参考文献
Fahrenholtz, Kenneth E.; Benz, Wolfgang; Blount, John F.; Williams, Thomas H.
Journal of Organic Chemistry, 1980 , vol. 45, # 21 p. 4219 - 4223
反应条件
in diethyl ether; water; triethylamine
1 h; Ambient temperature; Yield given;
参考文献
Fahrenholtz, Kenneth E.; Benz, Wolfgang; Blount, John F.; Williams, Thomas H.
Journal of Organic Chemistry, 1980 , vol. 45, # 21 p. 4219 - 4223
