乙酸-3-甲基-3-丁烯-1-醇酯合成路线 （共 36 条）
反应条件
trifluoroacetic acid in nitromethane T=0°C; 1.5 h; Yield given. Further byproducts given. Yields of byproduct given;
参考文献
Badet,B.; Julia,M.; Mallet,J.M.
Tetrahedron, 1988 , vol. 44, p. 2913
反应条件
N-ethyl-N,N-diisopropylamine T=70°C; 20 h; Yield given. Further byproducts given. Yields of byproduct given;
参考文献
Badet, B.; Julia, M.; Marazano, C.
Tetrahedron Letters, 1985 , vol. 26, # 16 p. 2007 - 2010
反应条件
N-ethyl-N,N-diisopropylamine T=70°C; 20 h; Yield given. Further byproducts given. Yields of byproduct given;
参考文献
Badet, B.; Julia, M.; Marazano, C.
Tetrahedron Letters, 1985 , vol. 26, # 16 p. 2007 - 2010
反应条件
N-ethyl-N,N-diisopropylamine T=70°C; 20 h; with other hintered amines too; Product distribution;
参考文献
Badet, B.; Julia, M.; Marazano, C.
Tetrahedron Letters, 1985 , vol. 26, # 16 p. 2007 - 2010
反应条件
1: 81 percent / HBF4 / CH2Cl2; diethyl ether / 0.5 h / -30 °C 2: t-BuOK / dimethylsulfoxide / 24 h / 20 °C View Scheme
参考文献
Tetrahedron, , vol. 44, p. 2913
反应条件
N-ethyl-N,N-diisopropylamine T=70°C; 20 h; Yield given. Further byproducts given. Yields of byproduct given;
参考文献
Badet, B.; Julia, M.; Marazano, C.
Tetrahedron Letters, 1985 , vol. 26, # 16 p. 2007 - 2010
反应条件
N-ethyl-N,N-diisopropylamine T=70°C; 20 h; with other hintered amines too; Product distribution;
参考文献
Badet, B.; Julia, M.; Marazano, C.
Tetrahedron Letters, 1985 , vol. 26, # 16 p. 2007 - 2010
反应条件
1: 68 percent / Zn(Cu) couple / diethyl ether / 6 h / Heating 2: 63 percent / Zn, AcOH / pyridine / 40 deg C, 2 h, then 70 deg C, 2 h 3: 85 percent / Ba(OH)2 / methanol / 0.5 h / 0 °C View Scheme
参考文献
Aljancic-Solaja, Ivana; Rey, Max; Dreiding, Andre S.
Helvetica Chimica Acta, 1987 , vol. 70, p. 1302 - 1306
反应条件
1: 68 percent / Zn(Cu) couple / diethyl ether / 6 h / Heating 2: 63 percent / Zn, AcOH / pyridine / 40 deg C, 2 h, then 70 deg C, 2 h View Scheme
参考文献
Aljancic-Solaja, Ivana; Rey, Max; Dreiding, Andre S.
Helvetica Chimica Acta, 1987 , vol. 70, p. 1302 - 1306
反应条件
3-chloro-benzenecarboperoxoic acid; zinc(II) chloride
1) i-PrNO2, -40 deg C than -10 deg C 40 min, 2) CH2Cl2, 1.5 h, -40 deg C; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Veselovskii, V. V.; Skorobogatov, S. P.; Novikova, M. A.; Moiseenkov, A. M.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1990 , vol. 39, # 3.1 p. 513 - 516
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1990 , # 3 p. 591 - 594
