反应条件
1: 1.) LiN(C3H7-i)2 / 1.) THF, hexamethylphosphoric triamide, -78 deg C, 75 min., 2.) -78 deg C, 1 h -> room temp., 1 h
2: 73 percent / Collins' reagent / CH2Cl2 / 0.58 h / Ambient temperature
View Scheme
参考文献
Smith, Amos B.; Levenberg, Patricia A.; Suits, Joan Z.
Synthesis, 1986 , # 3 p. 184 - 189
