4-[二(1H-吡咯-2-基)甲基]吡啶合成路线 (共 4 条)
反应条件
propionic acid 1.16667 h; Heating;
参考文献
Angewandte Chemie - International Edition, , vol. 46, # 23 p. 4320 - 4324
反应条件
1: With trifluoroacetic acid in dichloromethane
T=0°C; 0.333333 h; Inert atmosphere;
2: With 2,3-dicyano-5,6-dichloro-p-benzoquinone in dichloromethane
T=20°C; 1 h; Inert atmosphere; TemperatureTimeSolvent;
参考文献
Boccalon, Mariangela; Iengo, Elisabetta; Tecilla, Paolo
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 24 p. 4056 - 4067
反应条件
T=85°C; 15 h; Inert atmosphere;
参考文献
Boccalon, Mariangela; Iengo, Elisabetta; Tecilla, Paolo
Journal of the American Chemical Society, 2012 , vol. 134, # 50 p. 20310 - 20313
反应条件
trifluoroacetic acid
T=20°C; Condensation; 0.0833333 h;
参考文献
Ka, Jae-Won; Lee, Chang-Hee
Tetrahedron Letters, 2000 , vol. 41, # 23 p. 4609 - 4613