2-溴-４-硝基吡啶氮氧化物合成路线 （共 24 条）
反应条件
1: 56 percent / ethanol / 16 h / 70 - 80 °C
2: 70 percent / 2 h / Heating
3: 70 percent / H2O / 7 h / 120 - 130 °C
4: 66 percent / PCl3 / CHCl3 / 22 h / Heating
5: 85 percent / benzene / 2 h / Heating
View Scheme
参考文献
Moerkved, Eva H.; Cronyn, Marshall W.
Journal fuer Praktische Chemie (Leipzig), 1980 , vol. 322, # 2 p. 343 - 347
反应条件
1: 73 percent / ethanol / 1 h / 70 - 80 °C
2: 73 percent / 2 h / Heating
3: 84 percent / H2O / 120 - 130 °C
4: 73 percent / PCl3 / CHCl3 / 22 h / Heating
5: 76 percent / benzene / 0.5 h / 25 °C
View Scheme
参考文献
Moerkved, Eva H.; Cronyn, Marshall W.
Journal fuer Praktische Chemie (Leipzig), 1980 , vol. 322, # 2 p. 343 - 347
反应条件
1: 73 percent / ethanol / 1 h / 70 - 80 °C
2: 73 percent / 2 h / Heating
3: 84 percent / H2O / 120 - 130 °C
4: 73 percent / PCl3 / CHCl3 / 22 h / Heating
5: 81 percent / benzene / 17 h / 25 °C
View Scheme
参考文献
Moerkved, Eva H.; Cronyn, Marshall W.
Journal fuer Praktische Chemie (Leipzig), 1980 , vol. 322, # 2 p. 343 - 347
反应条件
1: 69 percent / ethanol / 3 h / 70 - 80 °C
2: 52 percent / 2 h / Heating
4: 66 percent / benzene / 17 h / Heating
View Scheme
参考文献
Moerkved, Eva H.; Cronyn, Marshall W.
Journal fuer Praktische Chemie (Leipzig), 1980 , vol. 322, # 2 p. 343 - 347
