bis(1,5-cyclooctadiene)-rhodium(I) tetrafluoroborate; 6-diphenylphosphinomethyl-3-methyl-2-aminopyridine in toluene T=150°C; 1 h; Inert atmosphere;

hydroxylamine hydrochloride; sodium acetate in ethanol 14 h; Heating;

<b>With</b>&nbsp; <a href="#" onclick="return RXDsubstances(event, this, '11604118', constants.ctx, '0')">tetrakis(triphenylphosphine) palladium⁽⁰⁾</a>;&nbsp;<a href="#" onclick="return RXDsubstances(event, this, '1911640', constants.ctx, '0')">2,6-di-tert-butyl-4-methyl-phenol</a>&nbsp;<b>in</b>&nbsp; <a href="#" onclick="return RXDsubstances(event, this, '635760', constants.ctx, '0')">toluene</a> <br />T=110&deg;C;&nbsp;16&nbsp;h;&nbsp;&nbsp;sealed tubeInert atmosphere;&nbsp;<br /> &nbsp;

<b>With</b>&nbsp; <a href="#" onclick="return RXDsubstances(event, this, '11342940', constants.ctx, '0')">sodium hydroxide</a> <br /> <br /> &nbsp;

<b>Multi-step reaction with 2 steps<br /> </b>1: 91 percent / n-BuLi / hexane; tetrahydrofuran / 1.) ice cooling, 30 min, 2.) room temperature, 14 h<br />2: n-BuLi / 1.) hexane, THF, -78 deg C, 0.5 h, 2.) -78 deg C, 1 h, room temperature, 1 h<br /> <br /> &nbsp;