苯基(吡啶-2-基)甲胺双盐酸盐合成路线 (共 2 条)
反应条件
1: With bis(η3-allyl-μ-chloropalladium(II)); cesium hydroxide monohydrate; tri-cyclo-hexyl-phosphine in anhydrous xylene
24 h; RefluxInert atmosphere;
2: With hydrogenchloride; sodium cyanoborohydride in ethanol; water
T=25°C; 2 h;
3: With hydrogenchloride in ethanol; water
T=25°C; 2 h;
参考文献
Niwa, Takashi; Suehiro, Takafumi; Yorimitsu, Hideki; Oshima, Koichiro
Tetrahedron, 2009 , vol. 65, # 26 p. 5125 - 5131
反应条件
hydrogenchloride in methanol; diethyl ether
T=20°C; 2 h; Inert atmosphere;
参考文献
Niwa, Takashi; Yorimitsu, Hideki; Oshima, Koichiro
Organic Letters, 2008 , vol. 10, # 20 p. 4689 - 4691