4-丙基-5,7-二羟基-6-(3-甲基-2-丁烯基)-8-(3-甲基丁酰)-2H-1-苯并吡喃-2-酮合成路线 （共 7 条）
反应条件
potassium hydroxide in water
T=0°C;
参考文献
Crombie; Jones; Palmer
Tetrahedron Letters, 1985 , vol. 26, # 24 p. 2929 - 2932
反应条件
1: 80 percent / AlCl3 / CS2; nitrobenzene / 0.5 h / Heating
2: cc. H2SO4 / acetic acid / 240 h / Ambient temperature
3: 23 percent / 10percent aq. potassium hydroxide / 1.5 h / 0 °C
View Scheme
参考文献
Crombie, Leslie; Jones, Raymond C. F.; Palmer, Christopher J.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1987 , p. 317 - 332
反应条件
1: cc. H2SO4 / acetic acid / 240 h / Ambient temperature
2: 23 percent / 10percent aq. potassium hydroxide / 1.5 h / 0 °C
View Scheme
参考文献
Crombie, Leslie; Jones, Raymond C. F.; Palmer, Christopher J.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1987 , p. 317 - 332
反应条件
1: 80 percent / AlCl3 / CS2; nitrobenzene / 0.5 h / Heating
2: cc. H2SO4 / acetic acid / 240 h / Ambient temperature
3: 23 percent / 10percent aq. potassium hydroxide / 1.5 h / 0 °C
View Scheme
参考文献
Crombie, Leslie; Jones, Raymond C. F.; Palmer, Christopher J.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1987 , p. 317 - 332
反应条件
potassium hydroxide
T=0°C; 1.5 h;
参考文献
Crombie, Leslie; Jones, Raymond C. F.; Palmer, Christopher J.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1987 , p. 317 - 332
反应条件
1: 66 percent / Sodium hydride(50percent in oil) / diethyl ether / 5 h / Heating
2: cc. H2SO4 / acetic acid / 240 h / Ambient temperature
3: 23 percent / 10percent aq. potassium hydroxide / 1.5 h / 0 °C
View Scheme
参考文献
Crombie, Leslie; Jones, Raymond C. F.; Palmer, Christopher J.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1987 , p. 317 - 332
反应条件
1: cc. H2SO4 / acetic acid / 240 h / Ambient temperature
2: 23 percent / 10percent aq. potassium hydroxide / 1.5 h / 0 °C
View Scheme
参考文献
Crombie, Leslie; Jones, Raymond C. F.; Palmer, Christopher J.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1987 , p. 317 - 332
