9-乙基-9-硼杂双环[3.3.1]壬烷合成路线 (共 4 条)
反应条件
in tetrahydrofuran stirring potassium borate (6.5 mmol) with 1,5-cyclooctandiylethylborate (8.9 mmol) in THF for 1 h at room temp.;; not isolated; detn. by (11B)-NMR;;
参考文献
Koester, Roland; Seidel, Guenter; Wagner, Klaus; Wrackmeyer, Bernd
Chemische Berichte, 1993 , vol. 126, # 2 p. 305 - 318
反应条件
2,6-di-tert-butyl-phenol; potassium tert-butylate in tetrahydrofuran
参考文献
Nambu,H.; Brown,H.C.
Journal of the American Chemical Society, 1970 , vol. 92, p. 5790 - 5791
反应条件
2,6-di-tert-butyl-phenol; potassium tert-butylate in tetrahydrofuran
参考文献
Nambu,H.; Brown,H.C.
Journal of the American Chemical Society, 1970 , vol. 92, p. 5790 - 5791
反应条件
palladium diacetate; O-(dicyclohexylphosphino)biphenyl in tetrahydrofuran
T=20°C; Suzuki coupling; 2 h;
参考文献
Crombie, Aimee L.; Kane Jr., John L.; Shea, Kevin M.; Danheiser, Rick L.
Journal of Organic Chemistry, 2004 , vol. 69, # 25 p. 8652 - 8667