1-(2-氯乙氧基)-2-甲氧基-4-甲基苯合成路线 (共 3 条)
反应条件
tetrachloromethane; triphenylphosphine in toluene
7 h; Heating;
参考文献
Kramer, Beate; Froehlich, Roland; Bergander, Klaus; Waldvogel, Siegfried R.
Synthesis, 2003 , # 1 p. 91 - 96
反应条件
1: 91 percent / K2CO3 / acetone / 4 h / Heating
2: 95 percent / NaBH4 / methanol / 0 °C
3: 67 percent / PPh3; CCl4 / toluene / 7 h / Heating
View Scheme
参考文献
Kramer, Beate; Froehlich, Roland; Bergander, Klaus; Waldvogel, Siegfried R.
Synthesis, 2003 , # 1 p. 91 - 96
反应条件
1: 95 percent / NaBH4 / methanol / 0 °C
2: 67 percent / PPh3; CCl4 / toluene / 7 h / Heating
View Scheme
参考文献
Kramer, Beate; Froehlich, Roland; Bergander, Klaus; Waldvogel, Siegfried R.
Synthesis, 2003 , # 1 p. 91 - 96