3'-碘-4'-甲基苯乙酮合成路线 （共 7 条）
反应条件
iodic acid in dichloromethane
T=20°C; 11 h;
参考文献
Chandrasekhar, Sosale; Gopalaiah, Kovuru
Tetrahedron Letters, 2002 , vol. 43, # 22 p. 4023 - 4024
反应条件
tris(trifluoroacetoxy)-λ3-iodane in dichloromethane
7 h; Ambient temperature;
参考文献
Fukuyama, Norihiro; Nishino, Hiroshi; Kurosawa, Kazu
Bulletin of the Chemical Society of Japan, 1987 , vol. 60, # 12 p. 4363 - 4368
反应条件
benzene
Erwaermen des Reaktionsprodukts mit wss.H2SO4 und Propionsaeure;
参考文献
Gore et al.
J.C.S.Perkin, vol. I, p. 1973 2940,2947
反应条件
aluminium trichloride
参考文献
Buu-Hoi; Jacquignon
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1957 , vol. 244, p. 786
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Gore et al.
J.C.S.Perkin, vol. I, p. 1973 2940,2944
反应条件
1: aq. NaOH
2: SOCl2
3: (i), (ii) (hydrolysis), (iii) (decarboxylation)
View Scheme
参考文献
Gore,P.H. et al.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1973 , p. 2940 - 2948
反应条件
1: SOCl2
2: (i), (ii) (hydrolysis), (iii) (decarboxylation)
View Scheme
参考文献
Gore,P.H. et al.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1973 , p. 2940 - 2948
反应条件
1: (i) NaNO2, aq. H2SO4, (ii) KI
2: aq. NaOH
3: SOCl2
4: (i), (ii) (hydrolysis), (iii) (decarboxylation)
View Scheme
参考文献
Gore,P.H. et al.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1973 , p. 2940 - 2948
