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结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
52182-93-1
合成路线
（共 13 条）
30673-29-1
→
反应条件
52182-93-1
反应条件
1: acetonitrile / 3 h / Ambient temperature; 1 eq. chloramine-B 2: acetonitrile / 3 h / Ambient temperature 3: H2O/silica gel / ethyl acetate 4: 58.2 percent / 30 h / Heating View Scheme
参考文献
Tomimatsu, Kiminori; Kataoka, Tadashi; Shimizu, Hiroshi; Hori, Mikio
Phosphorus and Sulfur and the Related Elements, 1983 , vol. 16, p. 97 - 110
124-41-4
甲醇钠
→
反应条件
52182-93-1
反应条件
in methanol 0.5 h; Ambient temperature;
参考文献
Tomimatsu, Kiminori; Kataoka, Tadashi; Shimizu, Hiroshi; Hori, Mikio
Phosphorus and Sulfur and the Related Elements, 1983 , vol. 16, p. 97 - 110
82238-25-3
→
反应条件
52182-93-1
反应条件
1: acetonitrile / 3 h / Ambient temperature 2: 83.8 percent / diethyl ether; benzene / 3 h / Heating 3: acetonitrile / 3 h / Ambient temperature; 1 eq. chloramine-T 4: 92 percent / H2O/silica gel / ethyl acetate 5: 58.2 percent / 30 h / Heating View Scheme
参考文献
Tomimatsu, Kiminori; Kataoka, Tadashi; Shimizu, Hiroshi; Hori, Mikio
Phosphorus and Sulfur and the Related Elements, 1983 , vol. 16, p. 97 - 110
82238-23-1
→
反应条件
52182-93-1
反应条件
1: 83.8 percent / diethyl ether; benzene / 3 h / Heating 2: acetonitrile / 3 h / Ambient temperature; 1 eq. chloramine-T 3: 92 percent / H2O/silica gel / ethyl acetate 4: 58.2 percent / 30 h / Heating View Scheme
参考文献
Tomimatsu, Kiminori; Kataoka, Tadashi; Shimizu, Hiroshi; Hori, Mikio
Phosphorus and Sulfur and the Related Elements, 1983 , vol. 16, p. 97 - 110
23974-72-3
→
反应条件
52182-93-1
反应条件
1: 86.1 percent / dimethylformamide / 4 h / 120 °C 2: 98.7 percent / diethyl ether / 1 h / Heating 3: 79.6 percent / 80percent H2SO4 / 0.5 h / 95 °C 4: acetonitrile / 3 h / Ambient temperature; 1 eq. chloramine-B 5: acetonitrile / 3 h / Ambient temperature 6: H2O/silica gel / ethyl acetate 7: 58.2 percent / 30 h / Heating View Scheme
参考文献
Tomimatsu, Kiminori; Kataoka, Tadashi; Shimizu, Hiroshi; Hori, Mikio
Phosphorus and Sulfur and the Related Elements, 1983 , vol. 16, p. 97 - 110
89-98-5
2-氯苯甲醛
→
反应条件
52182-93-1
反应条件
1: 86.1 percent / dimethylformamide / 4 h / 120 °C 2: 98.7 percent / diethyl ether / 1 h / Heating 3: 79.6 percent / 80percent H2SO4 / 0.5 h / 95 °C 4: acetonitrile / 3 h / Ambient temperature; 1 eq. chloramine-B 5: acetonitrile / 3 h / Ambient temperature 6: H2O/silica gel / ethyl acetate 7: 58.2 percent / 30 h / Heating View Scheme
参考文献
Tomimatsu, Kiminori; Kataoka, Tadashi; Shimizu, Hiroshi; Hori, Mikio
Phosphorus and Sulfur and the Related Elements, 1983 , vol. 16, p. 97 - 110
88048-84-4
→
反应条件
52182-93-1
反应条件
1: 98.7 percent / diethyl ether / 1 h / Heating 2: 79.6 percent / 80percent H2SO4 / 0.5 h / 95 °C 3: acetonitrile / 3 h / Ambient temperature; 1 eq. chloramine-B 4: acetonitrile / 3 h / Ambient temperature 5: H2O/silica gel / ethyl acetate 6: 58.2 percent / 30 h / Heating View Scheme
参考文献
Tomimatsu, Kiminori; Kataoka, Tadashi; Shimizu, Hiroshi; Hori, Mikio
Phosphorus and Sulfur and the Related Elements, 1983 , vol. 16, p. 97 - 110
88048-85-5
→
反应条件
52182-93-1
反应条件
1: 79.6 percent / 80percent H2SO4 / 0.5 h / 95 °C 2: acetonitrile / 3 h / Ambient temperature; 1 eq. chloramine-B 3: acetonitrile / 3 h / Ambient temperature 4: H2O/silica gel / ethyl acetate 5: 58.2 percent / 30 h / Heating View Scheme
参考文献
Tomimatsu, Kiminori; Kataoka, Tadashi; Shimizu, Hiroshi; Hori, Mikio
Phosphorus and Sulfur and the Related Elements, 1983 , vol. 16, p. 97 - 110
52183-06-9
+
922-67-8
甲基丙烯酸酯
→
反应条件
52182-93-1
+
30571-10-9
+
85891-62-9
反应条件
in dichloromethane 72 h; Heating; Further byproducts given;
参考文献
Kataoka, Tadashi; Tomimatsu, Kiminori; Shimizu, Hiroshi; Hori, Mikio
Chemical and Pharmaceutical Bulletin, 1984 , vol. 32, # 7 p. 2666 - 2675
82238-33-3
+
922-67-8
甲基丙烯酸酯
→
反应条件
52182-93-1
+
30571-10-9
+
85891-62-9
反应条件
in dichloromethane Heating; Further byproducts given;
参考文献
Kataoka, Tadashi; Tomimatsu, Kiminori; Shimizu, Hiroshi; Hori, Mikio
Tetrahedron Letters, 1983 , vol. 24, # 1 p. 75 - 78
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