2-甲基-2-(苯基硫代)丙酸合成路线 (共 6 条)
反应条件
1: With methanol; lithium hydroxide; water in tetrahydrofuran
T=20°C;
2: With hydrogenchloride in dihydrogen peroxide
pH=2;
参考文献
Yao, Wenqing; Zhang, Colin; He, Chunhong; Zhuo, Jincong
Patent: US2005/288329 A1, 2005 ;
Location in patent: Page/Page column 35 ;
US 20050288329 A1
反应条件
sodium hydroxide in chloroform; water; acetone
参考文献
Merck and Co., Inc.
Patent: US4864038 A1, 1989 ;
反应条件
sodium hydroxide
24 h; Ambient temperature;
参考文献
Kumaran, G.; Kulkarni, G. H.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1994 , vol. 33, # 2 p. 168 - 170
参考文献
Piechulek; Suszko
Roczniki Chemii, 1933 , vol. 13, p. 520,528
Chem. Zentralbl., 1934 , vol. 105, # I p. 2584
反应条件
ethanol
anschliessendes Erwaermen mit wss. Natronlauge;
参考文献
Fawcett et al.
Annals of Applied Biology, 1955 , vol. 43, p. 342,343, 344
Proceedings of the Royal Society of London, Series B: Biological Sciences, 1959 , vol. 150, p. 95,96, 100
反应条件
sulfuric acid
Heating;
参考文献
Andreani; Andrisano
Farmaco, Edizione Scientifica, 1975 , vol. 30, # 10 p. 847 - 858