(R)-(+)-1-(2-萘基)乙醇合成路线 （共 65 条）
反应条件
1,8-diazabicyclo[5.4.0]undec-7-ene in tetrahydrofuran T=20°C; Inert atmosphereAnhydrous conditions; optical yield given as percent eeenantioselective reaction;
参考文献
Leclercq, Loic; Suisse, Isabelle; Agbossou-Niedercorn, Francine
European Journal of Organic Chemistry, 2010 , # 14 p. 2696 - 2700
反应条件
in benzene T=20°C; 1.5 h; magnetic field B0 1.2;
参考文献
Zadel, Guido; Eisenbraun, Catja; Wolff, Gerd-Joachim; Breitmaier, Eberhard
Angewandte Chemie, 1994 , vol. 106, # 4 p. 460 - 463
反应条件
vinyl acetate; 4 Anstroem molecular sives; lipase LIP in di-isopropyl ether T=30°C; 0.5 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Kato; Katayama; Fujii; Kimoto
Bioscience, biotechnology, and biochemistry, 1995 , vol. 59, # 11 p. 2178 - 2180
反应条件
1,8-diazabicyclo[5.4.0]undec-7-ene in tetrahydrofuran T=20°C; Inert atmosphereAnhydrous conditions; optical yield given as percent ee;
参考文献
Leclercq, Loic; Suisse, Isabelle; Agbossou-Niedercorn, Francine
European Journal of Organic Chemistry, 2010 , # 14 p. 2696 - 2700
反应条件
(R)-(+)-N-methylbenzoguanidine; trimethylacetic anhydride in diethyl ether T=20°C; 12 h; Resolution of racemate; optical yield given as percent ee;
参考文献
Nakata, Kenya; Shiina, Isamu
Organic and Biomolecular Chemistry, 2011 , vol. 9, # 20 p. 7092 - 7096
反应条件
triphenylphosphine; diethylazodicarboxylate in dichloromethane T=-23 - 20°C; Mitsunobu reaction;
参考文献
Chandrasekhar, Sosale; Kulkarni, Guruprasad
Tetrahedron Asymmetry, 2002 , vol. 13, # 6 p. 615 - 619
反应条件
1: diethyl ether / 2 h / 0 °C / Inert atmosphere 2: C28H26N2O; triethylamine / 1,1-dimethylpropan-1-ol / 7 h / 0 °C / Inert atmosphere; Resolution of racemate View Scheme
参考文献
Crittall, Matthew R.; Rzepa, Henry S.; Carbery, David R.
Organic Letters, 2011 , vol. 13, # 5 p. 1250 - 1253
反应条件
(5aS,10bR)-5a,10b-dihydro-2-(pentafluorophenyl)-4H,6H-indeno[2,1-b][1,2,4]triazolo[4,3-d][1,4]oxazinium tetrafluoroborate; 3-benzylriboflavin tetraacetate; triethylamine in toluene T=20°C; 4 h; Resolution of racemateAirMolecular sieve; optical yield given as percent eeenantioselective reaction;
参考文献
Iwahana, Soichiro; Iida, Hiroki; Yashima, Eiji
Chemistry - A European Journal, 2011 , vol. 17, # 29 p. 8009 - 8013
反应条件
C32H31Cl2N4OPRu; potassium isopropoxide T=30°C; P=750.075 Torr; 0.333333 h; Inert atmosphere; optical yield given as percent eeenantioselective reaction;
参考文献
Ye, Wenjing; Zhao, Miao; Yu, Zhengkun
Chemistry - A European Journal, 2012 , vol. 18, # 35 p. 10843 - 10846
反应条件
Na-Pi buffer in acetone 48 h; tubers of Helianthus tuberosus presence, pH 5.9; other biologically active material: tubers of Solanum tuberosum cv. Saturna; Further byproducts given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Mironowicz, Agnieszka
Phytochemistry, 1998 , vol. 47, # 8 p. 1531 - 1534
