甲基(2E)-二氢-2(3H)-呋喃亚基乙酸酯合成路线 （共 16 条）
反应条件
in tetrahydrofuran
26 h;
参考文献
Bellur, Esen; Langer, Peter
Synlett, 2004 , # 12 p. 2169 - 2171
反应条件
1: 66 percent / NaH; n-BuLi / tetrahydrofuran; hexane / 15 h / -30 °C
2: 10 percent / I2; Na2HPO4; Na2SO4 / 90 h / 65 °C
View Scheme
参考文献
Calvet, Sandrine; David, Olivier; Vanucci-Bacque, Corinne; Fargeau-Bellassoued, Marie-Claude; Lhommet, Gerard
Tetrahedron, 2003 , vol. 59, # 33 p. 6333 - 6339
反应条件
1: 94 percent / n-BuLi / hexane; tetrahydrofuran / 2 h / -78 °C
2: 95 percent / PPTS / ethanol / 0.5 h / Heating
3: 74 percent / NaH / methanol / 0.5 h / Ambient temperature
View Scheme
参考文献
Pflieger, D.; Muckensturm, B.
Tetrahedron, 1989 , vol. 45, # 7 p. 2031 - 2040
反应条件
1: 82 percent / PPTS / CH2Cl2 / Ambient temperature
2: 94 percent / n-BuLi / hexane; tetrahydrofuran / 2 h / -78 °C
3: 95 percent / PPTS / ethanol / 0.5 h / Heating
4: 74 percent / NaH / methanol / 0.5 h / Ambient temperature
View Scheme
参考文献
Pflieger, D.; Muckensturm, B.
Tetrahedron, 1989 , vol. 45, # 7 p. 2031 - 2040
反应条件
1: 95 percent / PPTS / ethanol / 0.5 h / Heating
2: 74 percent / NaH / methanol / 0.5 h / Ambient temperature
View Scheme
参考文献
Pflieger, D.; Muckensturm, B.
Tetrahedron, 1989 , vol. 45, # 7 p. 2031 - 2040
反应条件
in tetrahydrofuran; hexane
-78 deg C, 1.5 h; 0 deg C, 1.5 h;
参考文献
Sauve, G.; Deslongchamps, P.
Synthetic Communications, 1985 , vol. 15, # 3 p. 201 - 212
