3-氨基-2-环己烯-1-酮合成路线 (共 56 条)
反应条件
in N,N-dimethyl-formamide
参考文献
US4762843 A1, ;
US 4762843 A
反应条件
acetic acid in toluene Addition; cyclization; Heating;
参考文献
Journal of Heterocyclic Chemistry, , vol. 37, # 1 p. 41 - 46
反应条件
1: 24 percent / ethanol / 2 h / Heating 2: 65 percent / diphenyl ether / 0.5 h / Heating View Scheme
参考文献
Gatta, Franco; Giudice, Maria Rosaria Del; Pomponi, Massimo; Marta, Maurizio
Heterocycles, 1992 , vol. 34, # 5 p. 991 - 1004
反应条件
1: 1-amino-1-cyclohexen-3-one With sodium hydride in N,N-dimethyl-formamide T=0°C; Metallation; 0.5 h; 2: di-tert-butyl dicarbonate in N,N-dimethyl-formamide T=0 - 23°C; Acylation; 0.5 h;
参考文献
Shepard, Mary S.; Carreira, Erick M.
Tetrahedron, 1997 , vol. 53, # 48 p. 16253 - 16276
参考文献
Shono, Tatsuya; Matsumura, Yoshihiro; Kashimura, Shigenori
Journal of Organic Chemistry, 1981 , vol. 46, # 18 p. 3719
参考文献
E. I. du Pont de Nemours and Company
Patent: US5202488 A1, 1993 ;
反应条件
mercury(II) diacetate in acetonitrile 20 h; Heating;
参考文献
Synthesis, , # 6 p. 471 - 472
参考文献
Shono, Tatsuya; Matsumura, Yoshihiro; Kashimura, Shigenori
Journal of Organic Chemistry, 1981 , vol. 46, # 18 p. 3719
参考文献
Mitsui Toatsu Chemicals, Incorporated
Patent: US5112817 A1, 1992 ;
反应条件
acetic acid in acetonitrile Cyclization; Heating;
参考文献
Singh, Kamaljit; Singh, Jasbir; Singh, Harjit
Tetrahedron, 1998 , vol. 54, # 5-6 p. 935 - 942