3-甲氧基苯基甲烷磺酸酯合成路线 （共 12 条）
反应条件
tetrabutyl ammonium fluoride; palladium diacetate; 2-(dicyclohexylphosphino)-2',4',6'-tri-i-propyl-1,1’-biphenyl in tetrahydrofuran; tert-butyl alcohol T=90°C; Hiyama coupling; Inert atmosphere;
参考文献
Organic Letters, , vol. 10, # 21 p. 4971 - 4974
反应条件
tetrabutyl ammonium fluoride; palladium diacetate; 2-(dicyclohexylphosphino)-2',4',6'-tri-i-propyl-1,1’-biphenyl in tetrahydrofuran; tert-butyl alcohol T=90°C; Hiyama coupling; Inert atmosphere;
参考文献
Organic Letters, , vol. 10, # 21 p. 4971 - 4974
反应条件
palladium diacetate; cesium fluoride; 2-(dicyclohexylphosphino)-2',4',6'-tri-i-propyl-1,1’-biphenyl in tert-butyl alcohol T=110°C; Stille coupling; 14 h; Inert atmosphere;
参考文献
Heterocycles, , vol. 80, # 2 p. 1215 - 1226
反应条件
t-Bu Brett Phos; water; palladium diacetate; caesium carbonate in tert-butyl alcohol T=110°C; 0.333333 h; Inert atmosphere;
参考文献
Dooleweerdt, Karin; Fors, Brett P.; Buchwald, Stephen L.
Organic Letters, 2010 , vol. 12, # 10 p. 2350 - 2353
反应条件
tetrabutyl ammonium fluoride; palladium diacetate; 2-(dicyclohexylphosphino)-2',4',6'-tri-i-propyl-1,1’-biphenyl in tetrahydrofuran; tert-butyl alcohol
T=90°C; Hiyama coupling; Inert atmosphere;
参考文献
Zhang, Liang; Qing, Jiang; Yang, Pengyuan; Wu, Jie
Organic Letters, 2008 , vol. 10, # 21 p. 4971 - 4974
反应条件
CM-phos; H2O4P(1-)*3K(1+); palladium diacetate; triethylamine in tert-butyl alcohol
T=20 - 110°C; Suzuki-Miyaura coupling; Inert atmosphere;
参考文献
Chow, Wing Kin; So, Chau Ming; Lau, Chak Po; Kwong, Fuk Yee
Journal of Organic Chemistry, 2010 , vol. 75, # 15 p. 5109 - 5112
反应条件
1,1'-bis-(diphenylphosphino)ferrocene; potassium phosphate; n-butyllithium; 1,1'-bis(diphenylphosphanyl)ferrocenenickel(II) chloride; potassium iodide
1.) toluene, room temperature, 30 min, 2.) toluene, 80 deg C, 16 h; Yield given. Multistep reaction;
参考文献
Ueda, Masato; Saitoh, Atsushi; Oh-tani, Saori; Miyaura, Norio
Tetrahedron, 1998 , vol. 54, # 43 p. 13079 - 13086
反应条件
potassium phosphate; trans-[Ni(Naph)Cl(PPh3)2]; tri-cyclo-hexyl-phosphine in tetrahydrofuran
T=25°C; Suzuki coupling; 12 h; Inert atmosphere;
参考文献
Leowanawat, Pawaret; Zhang, Na; Safi, Mehtap; Hoffman, David J.; Fryberger, Miriam C.; George, Aiswaria; Percec, Virgil
Journal of Organic Chemistry, 2012 , vol. 77, # 6 p. 2885 - 2892
反应条件
lithium chloride; copper(l) iodide; tris(dibenzylideneacetone)dipalladium (0) in N,N-dimethyl-formamide
T=80°C; 2 h;
参考文献
Badone, Domenico; Cardamone, Rosanna; Guzzi, Umberto
Tetrahedron Letters, 1994 , vol. 35, # 30 p. 5477 - 5480
反应条件
pyridine in dichloromethane
T=0 - 20°C; Inert atmosphere;
参考文献
Song, Bingrui; Knauber, Thomas; Goossen, Lukas J.
Angewandte Chemie - International Edition, 2013 , vol. 52, # 10 p. 2954 - 2958
Angew. Chem., 2013 , vol. 125, # 10 p. 3026 - 3030
