N1-(4-吡啶基)苯甲酰胺合成路线 （共 11 条）
反应条件
CyPF-t-Bu; sodium t-butanolate; palladium diacetate in ethylene glycol dimethyl ether T=70°C; 24 h;
参考文献
Shen, Qilong; Shekhar, Shashank; Stambuli, James P.; Hartwig, John F.
Angewandte Chemie - International Edition, 2005 , vol. 44, # 9 p. 1371 - 1375
反应条件
sodium t-butanolate; palladium diacetate; CyPF-t-Bu in ethylene glycol dimethyl ether T=70°C; 10 h;
参考文献
Shen, Qilong; Ogata, Tokutaro; Hartwig, John F.
Journal of the American Chemical Society, 2008 , vol. 130, # 20 p. 6586 - 6596
反应条件
0.0166667 h; microwave irradiation;
参考文献
Li, Yanqiu; Wang, Yulu; Wang, Jinye
Heterocyclic Communications, 2007 , vol. 13, # 4 p. 251 - 256
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Li, Yanqiu; Wang, Yulu; Wang, Jinye
Russian Journal of Organic Chemistry, 2008 , vol. 44, # 3 p. 358 - 361
反应条件
1: 4-amino-pyridine With n-butyllithium in tetrahydrofuran; hexane T=20°C; 1 h; 2: benzoyl-protected allyl alcohol in tetrahydrofuran; hexane T=20°C; 12 h;
参考文献
Faler, Catherine A.; Joullie, Madeleine M.
Tetrahedron Letters, 2006 , vol. 47, # 40 p. 7229 - 7231
反应条件
triethylamine in acetonitrile T=20°C; Acetylation; 2 h;
参考文献
Bakke; Riha
Journal of Heterocyclic Chemistry, 1999 , vol. 36, # 5 p. 1143 - 1145
反应条件
sodium carbonate in acetonitrile 2.5 h; Irradiation;
参考文献
Park; Jung; Kim; Song
Journal of Organic Chemistry, 2001 , vol. 66, # 7 p. 2197 - 2206
反应条件
1: 69 percent / acetonitrile 2: 37 percent / aq. Na2CO3 / acetonitrile / 2.5 h / Irradiation View Scheme
参考文献
Park; Jung; Kim; Song
Journal of Organic Chemistry, 2001 , vol. 66, # 7 p. 2197 - 2206
反应条件
1: 69 percent / acetonitrile 2: 37 percent / aq. Na2CO3 / acetonitrile / 2.5 h / Irradiation View Scheme
参考文献
Park; Jung; Kim; Song
Journal of Organic Chemistry, 2001 , vol. 66, # 7 p. 2197 - 2206
反应条件
1.1: 87 percent / thionyl chloride / 0 - 20 °C 2.1: n-butyl lithium / hexane; tetrahydrofuran / 1 h / 20 °C 2.2: 86 percent / hexane; tetrahydrofuran / 12 h / 20 °C View Scheme
参考文献
Faler, Catherine A.; Joullie, Madeleine M.
Tetrahedron Letters, 2006 , vol. 47, # 40 p. 7229 - 7231
反应条件
in 1-methyl-pyrrolidin-2-one T=50°C; 114 h; Inert atmosphere; Kinetics; Time;
参考文献
Woodman, Emily K.; Chaffey, Julian G. K.; Hopes, Philip A.; Hose, David R. J.; Gilday, John P.
Organic Process Research and Development, 2009 , vol. 13, # 1 p. 106 - 113
