2-溴-3',5'-二特戊酰氧基苯乙酮合成路线 （共 4 条）
反应条件
pyridinium bromide perbromate in acetic acid
T=20°C; 1 h;
参考文献
Reddy, Indra K.; Vaithiyalingam, Siva R.; Khan, Mansoor A.; Bodor, Nicholas S.
Journal of Pharmaceutical Sciences, 2001 , vol. 90, # 8 p. 1026 - 1033
反应条件
1: 77 percent / pyridine / 5 h / 20 °C
2: 67 percent / pyridinium bromide perbromate / acetic acid / 1 h / 20 °C
View Scheme
参考文献
Reddy, Indra K.; Vaithiyalingam, Siva R.; Khan, Mansoor A.; Bodor, Nicholas S.
Journal of Pharmaceutical Sciences, 2001 , vol. 90, # 8 p. 1026 - 1033
反应条件
1: 77 percent / pyridine / 5 h / 20 °C
2: 67 percent / pyridinium bromide perbromate / acetic acid / 1 h / 20 °C
View Scheme
参考文献
Reddy, Indra K.; Vaithiyalingam, Siva R.; Khan, Mansoor A.; Bodor, Nicholas S.
Journal of Pharmaceutical Sciences, 2001 , vol. 90, # 8 p. 1026 - 1033
反应条件
(i) Et3N, CHCl3, (ii) Br2, AlCl3, AcOtBu; Multistep reaction;
参考文献
ICI
Patent: BE861894DE2756001 , 19781978 ;
Chem.Abstr., 1978 , vol. 89, # 129233
