4-甲基-beta-甲基-beta-硝基苯乙烯合成路线 （共 13 条）
反应条件
2-HEAF T=20°C; Knoevenagel condensation; 4.1 h; Ionic liquid;
参考文献
Alizadeh, Abdolhamid; Khodaei, Mohammad M.; Eshghi, Ali
Journal of Organic Chemistry, 2010 , vol. 75, # 23 p. 8295 - 8298
反应条件
methanesulfonyl chloride; N-ethyl-N,N-diisopropylamine in dichloromethane T=20°C; Inert atmosphereCooling with ice;
参考文献
Agut, Juan; Vidal, Andreu; Rodriguez, Santiago; Gonzalez, Florenci V.
Journal of Organic Chemistry, 2013 , vol. 78, # 11 p. 5717 - 5722
反应条件
1: triethylamine / 16 h / 20 °C / |Inert atmosphere 2: N-ethyl-N,N-diisopropylamine; methanesulfonyl chloride / dichloromethane / 20 °C / |Inert atmosphere; |Cooling with ice View Scheme
参考文献
Agut, Juan; Vidal, Andreu; Rodriguez, Santiago; Gonzalez, Florenci V.
Journal of Organic Chemistry, 2013 , vol. 78, # 11 p. 5717 - 5722
反应条件
in acetonitrile T=30°C; var. temp.; Equilibrium constant;
参考文献
Shunmugasundaram, A; Thanulingam, T Lekshmana; Murugesan, R
Indian Journal of Chemistry, Section A: Inorganic, Bio-inorganic, Physical, Theoretical & Analytical Chemistry, 1991 , vol. 30, # 7 p. 609 - 613
反应条件
hydrogenchloride; iron; iron(II) chloride in ethanol
参考文献
Aizpurua, J. M.; Oiarbide, M.; Palomo, C.
Tetrahedron Letters, 1987 , vol. 28, # 44 p. 5365 - 5366
反应条件
potassium carbonate in tetrahydrofuran 10 h; Ambient temperature;
参考文献
Bulletin de la Societe Chimique de France, , # 4 p. 562 - 565
反应条件
potassium carbonate in tetrahydrofuran 10 h; Ambient temperature;
参考文献
Bulletin de la Societe Chimique de France, , # 4 p. 562 - 565
反应条件
potassium carbonate in tetrahydrofuran 10 h; Ambient temperature;
参考文献
Bulletin de la Societe Chimique de France, , # 4 p. 562 - 565
反应条件
anhydrous iron chloride in ethylene glycol T=100°C; 6 h;
参考文献
Li, Liang; Zhao, Mi-Na; Ren, Zhi-Hui; Li, Jianli; Guan, Zheng-Hui
Synthesis, 2012 , vol. 44, # 4 p. 532 - 540
反应条件
hydrogenchloride; potassium hydroxide
1) ether, reflux, 2) methanol, water, 0.5 h, reflux; Yield given. Multistep reaction;
参考文献
Boberg, Friedrich; Garburg, Karl-Heinz; Goerlich, Karl-Joachim; Pipereit, Eberhard; Ruhr, Maria
Liebigs Annalen der Chemie, 1985 , # 2 p. 239 - 250
