4-甲氧基-2甲基苯甲醛合成路线 （共 35 条）
反应条件
sodium hydroxide in water
参考文献
Akguen, Eyup; Glinski, Margaret B.; Dhawan, Kasturi L.; Durst, Tony
Journal of Organic Chemistry, 1981 , vol. 46, # 13 p. 2730 - 2734
反应条件
1: 100 percent / LiAlH4, Celite / tetrahydrofuran / 2 h / 0 - 20 °C 2: 93 percent / PCC, Celite, florosil / CH2Cl2 / 1.3 h / Ambient temperature View Scheme
参考文献
Shishido KJ.; Yamashita; Hiroya; Fukumoto; Kametani
Tetrahedron Letters, 1989 , vol. 30, # 1 p. 111 - 112
反应条件
1: 97 percent / potassium carbonate / acetone / 19 h / Heating 2: 100 percent / LiAlH4, Celite / tetrahydrofuran / 2 h / 0 - 20 °C 3: 93 percent / PCC, Celite, florosil / CH2Cl2 / 1.3 h / Ambient temperature View Scheme
参考文献
Shishido KJ.; Yamashita; Hiroya; Fukumoto; Kametani
Tetrahedron Letters, 1989 , vol. 30, # 1 p. 111 - 112
反应条件
1: n-BuLi, MgBr2 / tetrahydrofuran; diethyl ether; hexane / -78 °C / warming to room temperature 2: NaOH / H2O View Scheme
参考文献
Dhawan, Kasturi L.; Gowland, Barbara D.; Durst, Tony
Journal of Organic Chemistry, 1980 , vol. 45, # 5 p. 922 - 924
参考文献
Sen, P. K.; Pal, Panchanan; Goswami, Shyamaprosad; Chattopadhyay, Gautam
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1987 , vol. 26, p. 679 - 682
反应条件
air; Titanium(IV) oxide; silver sulphate in water; acetonitrile Oxidation; oxygenation; 2 h; Irradiation;
参考文献
Ranchella, Michele; Rol, Cesare; Sebastiani, Giovanni V.
Journal of the Chemical Society. Perkin Transactions 2, 2000 , # 2 p. 311 - 315
反应条件
1: HCl, AlCl3 / benzene View Scheme
参考文献
Laarhoven,W.H. et al.
Recueil des Travaux Chimiques des Pays-Bas, 1961 , vol. 80, p. 775 - 791
反应条件
sodium hydrogencarbonate; silver nitrate; triethylamine 1.) DMSO, room temp, 1 h, 2.) 15 min; Yield given. Multistep reaction;
参考文献
Ghera, E.; Plemenitas, A.; Ben-David, Y.
Synthesis, 1984 , # 6 p. 504 - 506
参考文献
Laarhoven,W.H. et al.
Recueil des Travaux Chimiques des Pays-Bas, 1961 , vol. 80, p. 775 - 791
反应条件
hydrogenchloride; aluminium trichloride Durch Zersetzen des Reaktionsproduktes durch Kochen mit verd. Salzsaeure;
参考文献
Gattermann
Chemische Berichte, 1898 , vol. 31, p. 1151
Justus Liebigs Annalen der Chemie, 1907 , vol. 357, p. 347
Full Text Show Details
Perkin; Weizmann
Journal of the Chemical Society, 1906 , vol. 89, p. 1651
