4-甲氧基-2甲基苯甲醛合成路线 （共 35 条）
反应条件
2: ethanolic KOH View Scheme
参考文献
Buu-Hoi et al.
Journal of Organic Chemistry, 1956 , vol. 21, p. 415,417, 418
反应条件
1: 79 percent / NaBH4 / ethanol / 2 h / 20 °C 2: thionyl chloride; DMF / CH2Cl2 / 3 h / 20 °C 3: 23 percent / ethanol / 3.5 h / Heating View Scheme
参考文献
Meyers; Sun; Carlson; Marriner; Katzenellenbogen
Journal of Medicinal Chemistry, 2001 , vol. 44, # 24 p. 4230 - 4251
反应条件
1: 60 percent / Jones' reagent
2: 1) oxalyl chloride
3: 62.5 percent / 1) silver oxide, 2) aq. sodium hydroxide (40percent) / methanol / 1) reflux, 2.5 hr, 2) reflux, 2 hr
View Scheme
参考文献
Sen, P. K.; Pal, Panchanan; Goswami, Shyamaprosad; Chattopadhyay, Gautam
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1987 , vol. 26, p. 679 - 682
反应条件
Yield given. Multistep reaction;
参考文献
Shishido KJ.; Yamashita; Hiroya; Fukumoto; Kametani
Tetrahedron Letters, 1989 , vol. 30, # 1 p. 111 - 112
反应条件
sodium tetrahydroborate in ethanol
T=20°C; 2 h;
参考文献
Meyers; Sun; Carlson; Marriner; Katzenellenbogen
Journal of Medicinal Chemistry, 2001 , vol. 44, # 24 p. 4230 - 4251
