2,2-二甲基-2,6-二氢-吡喃并[3,2-c]喹啉-5-酮合成路线 (共 37 条)
反应条件
potassium permanganate; acetone
Erwaermen des nach Ansaeuern mit wss. H3PO4 erhaltenen Reaktionsprodukts mit Aethanol;
参考文献
Brown et al.
Australian Journal of Chemistry, 1954 , vol. 7, p. 348,369
反应条件
potassium carbonate in N,N-dimethyl-formamide
T=20°C; 10 h;
参考文献
Wang, Xue; Yong, Rok Lee
Synthesis, 2007 , # 19 p. 3044 - 3050
反应条件
2,3-dicyano-5,6-dichloro-p-benzoquinone in benzene
4 h; Heating;
参考文献
Ramesh, M.; Mohan, P. S.; Shanmugam, P.
Tetrahedron, 1984 , vol. 40, # 20 p. 4041 - 4050
反应条件
2,3-dicyano-5,6-dichloro-p-benzoquinone in benzene
15 h; Heating;
参考文献
Suresh; Dhanabal; Nandha Kumar; Mohan
Heterocyclic Communications, 2005 , vol. 11, # 1 p. 79 - 84
反应条件
water
T=80°C; Domino Knoevenagel/6π-electrocyclization; 6 h;
参考文献
Jung, Ene Jin; Park, Byung Ho; Lee, Yong Rok
Green Chemistry, 2010 , vol. 12, # 11 p. 2003 - 2011
反应条件
sodium hydroxide; N-benzyl-N,N,N-triethylammonium chloride in toluene
T=50°C; 88 h; MechanismProduct distribution;
参考文献
Reisch, Johannes; Bathe, Andreas; Salehi-Artimani, Reza A.
Archiv der Pharmazie (Weinheim, Germany), 1986 , vol. 319, # 8 p. 720 - 727
反应条件
2,3-dicyano-5,6-dichloro-p-benzoquinone in benzene
12 h; Heating;
参考文献
Ramesh, M.; Mohan, P. S.; Shanmugam, P.
Tetrahedron, 1984 , vol. 40, # 20 p. 4041 - 4050
反应条件
ethylenediamine diacetic acid in dichloromethane
T=20°C; 10 h; Product distribution; Further Variations:ReagentsSolventsTemperaturesreaction times;
参考文献
Wang, Xue; Yong, Rok Lee
Synthesis, 2007 , # 19 p. 3044 - 3050
反应条件
pyridine; trichlorophosphate
1.5 h; Heating;
参考文献
Anand, R C; Sinha, A K
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1991 , vol. 30, # 6 p. 560 - 562
反应条件
1: 67 percent / polyphosphoric acid / xylene / 10 h / 20 - 145 °C
2: 85 percent / DDQ / benzene / 12 h / Heating
View Scheme
参考文献
Thangavel, Dhanabal; Ravindran, Sangeetha; Moonsamy, Gengan Robert; Palathurai, Mohan Subramaniam
Journal of Chemical Research, 2007 , # 2 p. 124 - 126