3-乙氧基羰基-1-苯基戊烷-1,4-二酮合成路线 （共 29 条）
参考文献
Cusmano
Gazzetta Chimica Italiana, 1939 , vol. 69, p. 214,218
反应条件
ethanol; sodium acetate und Erwaermen des Reaktionsprodukts mit wss.NaOH;
参考文献
Finar
Journal of the Chemical Society, 1955 , p. 1205,1207
反应条件
[BMIm][HSO4] T=150°C; Paal-Knorr furan synthesis; 3 h; Sealed tubeNeat (no solvent);
参考文献
Wang, Gangqiang; Guan, Zhi; Tang, Rongchang; He, Yanhong
Synthetic Communications, 2010 , vol. 40, # 3 p. 370 - 377
反应条件
1: 80 percent / Na2CO3 / methanol; H2O / 6 h / Heating 2: 90 percent / zinc chloride, acetic anhydride / 3 h / 85 °C View Scheme
参考文献
Mackay, Donald; Dao, Le H.; Dust, Julian M.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 2408 - 2416
参考文献
Paal
Chemische Berichte, 1884 , vol. 17, p. 2766
Chemische Berichte, 1885 , vol. 18, p. 58
反应条件
1: aqueous HNO3 2: aq.-ethanolic NaOH View Scheme
参考文献
Cusmano; Massara
Gazzetta Chimica Italiana, 1938 , vol. 68, p. 566,568
反应条件
1: 72 percent / 12 M hydrochloric acid / ethanol / 24 h / Heating 2: 35 percent / pieces of sodium / ethanol / 3 h / Heating View Scheme
参考文献
Farmaco, Edizione Scientifica, , vol. 42, # 5 p. 629 - 639
反应条件
ammonium acetate; silica gel
T=70°C; Paal-Knorr pyrrole synthesis; 0.5 h; Infrared heatingNeat (no solvent);
参考文献
Zhang, Chun; Wang, Jian; Li, Jing-Hua
Journal of Heterocyclic Chemistry, 2012 , vol. 49, # 1 p. 204 - 207
反应条件
toluene-4-sulfonic acid in diethyl ether; ethanol
参考文献
ICOS Corporation
Patent: US6372777 B1, 2002 ;
反应条件
1: 60 percent / acetic acid / 1 h / 80 °C / Heating
2: 95 percent / aq. NaOH / ethanol / 24 h / 50 °C
View Scheme
参考文献
Petruso, S.; Caronna, S.; Sferlazzo, M.; Sprio, V.
Journal of Heterocyclic Chemistry, 1990 , vol. 27, # 5 p. 1277 - 1280
