1: 1-[(Methylethyl)thio]-4-fluorobenzene With n-butyllithium in tetrahydrofuran; hexane
T=-85°C; Metallation; 6 h;
2: methyl iodide in tetrahydrofuran; hexane
T=20°C; Methylation; 3 h; Title compound not separated from byproducts;
参考文献
Cabiddu; Cadoni; Fattuoni; Melis
Journal of Fluorine Chemistry, 1999 , vol. 98, # 2 p. 97 - 106