2-甲酰基-3,5-二甲氧基苯甲酸甲酯合成路线 （共 8 条）
反应条件
potassium carbonate in acetone
参考文献
Talapatra, Bani; Roy, Monoj K.; Talapatra, Sunil K.
Journal of the Indian Chemical Society, 1983 , vol. 60, p. 1169 - 1171
反应条件
trichlorophosphate T=0 - 20°C; Vilsmeier-Haack reaction; 4.5 h;
参考文献
Srivastava, Vandana; Darokar, Mahendra P.; Fatima, Atiya; Kumar; Chowdhury, Chinmay; Saxena, Hari Om; Dwivedi, Gaurav R.; Shrivastava, Kunal; Gupta, Vivek; Chattopadhyay; Luqman, Suaib; Gupta; Negi, Arvind S.; Khanuja, Suman P.S.
Bioorganic and Medicinal Chemistry, 2007 , vol. 15, # 1 p. 518 - 525
反应条件
potassium carbonate; acetone
参考文献
Kamal et al.
Journal of the Chemical Society, 1950 , p. 3375,3378
反应条件
titanium tetrachloride Addition;
参考文献
Murty; Hazra; Datta; Mal
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 1997 , vol. 36, # 2 p. 126 - 132
反应条件
hydrogenchloride in methanol Cyclization; 5 h; Heating;
参考文献
Murty; Hazra; Datta; Mal
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 1997 , vol. 36, # 2 p. 126 - 132
反应条件
1,1-diethyl-3-(3'-indolyl)-(2S)-(N-methyl-N-3'',3''-dimethylbutylamino)-1-propanol in hexane; toluene T=-15°C; 10 h; Inert atmosphere;
参考文献
Ren, Jie; Jiang, Ju-Xing; Li, Ang-Bo; Liao, Tou-Geng; Tian, Ren-Rong; Chen, Xu-Lin; Jiang, Si-Ping; Pittman Jr., Charles U.; Zhu, Hua-Jie
European Journal of Organic Chemistry, 2009 , # 23 p. 3987 - 3991
反应条件
1: 65 percent / KMnO4, MgSO4 / H2O; acetone / 1 h / Heating 2: 60 percent / LiAlH4 / diethyl ether / 1 h / Heating 3: 38 percent / BBr3 / CH2Cl2 / 28 h / Ambient temperature View Scheme
参考文献
Talapatra, Bani; Roy, Monoj K.; Talapatra, Sunil K.
Journal of the Indian Chemical Society, 1983 , vol. 60, p. 1169 - 1171
反应条件
1: 65 percent / KMnO4, MgSO4 / H2O; acetone / 1 h / Heating
2: 60 percent / LiAlH4 / diethyl ether / 1 h / Heating
3: 60 percent / AlCl3 / CH2Cl2 / 1.5 h / Heating
View Scheme
参考文献
Talapatra, Bani; Roy, Monoj K.; Talapatra, Sunil K.
Journal of the Indian Chemical Society, 1983 , vol. 60, p. 1169 - 1171
