1,4-二乙酰氧基-2-溴苯合成路线 (共 7 条)
反应条件
bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triphenylphosphine 10 h; Heating / reflux;
参考文献
FUJI PHOTO FILM CO., LTD.
Patent: WO2005/85222 A1, 2005 ;
Location in patent: Page/Page column 83-84 ;
反应条件
bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triphenylphosphine
10 h; Heating / reflux;
参考文献
FUJI PHOTO FILM CO., LTD.
Patent: WO2005/85222 A1, 2005 ;
Location in patent: Page/Page column 83-84 ;
参考文献
Schulz,H.
Chemische Berichte, 1882 , vol. 15, p. 656
反应条件
zinc dibromide
T=100°C; 3 h;
参考文献
Pulley, Shon R.; Czako, Barbara
Tetrahedron Letters, 2004 , vol. 45, # 28 p. 5511 - 5514
反应条件
N,N,N',N,-tetramethylethylenediamine in tetrahydrofuran
T=20°C;
参考文献
Bochicchio, Antonella; Chiummiento, Lucia; Funicello, Maria; Lopardo, Maria Teresa; Lupattelli, Paolo
Tetrahedron Letters, 2010 , vol. 51, # 21 p. 2824 - 2827
反应条件
pyridine; boron tribromide
Yield given. Yields of byproduct given;
参考文献
Garst, Michael E.; Frazier, Janice D.
Journal of Organic Chemistry, 1987 , vol. 52, # 3 p. 446 - 448
参考文献
Schulz,H.
Chemische Berichte, 1882 , vol. 15, p. 656