2,5-二甲基-3-硝基吡啶合成路线 (共 3 条)
反应条件
hydrogen; palladium on activated charcoal in methanol
T=20°C; 15 h;
参考文献
ISHIHARA SANGYO KAISHA, LTD.
Patent: WO2009/88103 A1, 2009 ;
Location in patent: Page/Page column 17 ;
反应条件
potassium carbonate; tetrakis(triphenylphosphine) palladium(0) in 1,4-dioxane
7.5 h; Inert atmosphereReflux;
参考文献
ISHIHARA SANGYO KAISHA, LTD.
Patent: WO2009/88103 A1, 2009 ;
Location in patent: Page/Page column 17 ;
反应条件
dinitrogen pentaoxide in liquid sulphur dioxide
T=-30°C; Yield given. Yields of byproduct given;
参考文献
Bakke, Jan M.; Hegbom, Ingrid; Oevreeide, Elin; Aaby, Kjersti
Acta Chemica Scandinavica, 1994 , vol. 48, # 12 p. 1001 - 1006