diisobutylaluminium hydride in toluene
T=-60°C; 2 h;
参考文献
Hitchcock, Stephen A.; Houldsworth, Stephen J.; Pattenden, Gerald; Pryde, David C.; Thomson, Nicholas M.; Blake, Alexander J.
Journal of the Chemical Society - Perkin Transactions 1, 1998 , # 19 p. 3181 - 3206
Hitchcock, Stephen A.; Houldsworth, Stephen J.; Pattenden, Gerald; Pryde, David C.; Thomson, Nicholas M.; Blake, Alexander J.
Journal of the Chemical Society - Perkin Transactions 1, 1998 , # 19 p. 3181 - 3206
1: 73 percent / K2CO3 / acetone / 24 h / Ambient temperature
2: 92 percent / DIBAL-H / toluene / 2 h / -60 °C
View Scheme
参考文献
Hitchcock, Stephen A.; Houldsworth, Stephen J.; Pattenden, Gerald; Pryde, David C.; Thomson, Nicholas M.; Blake, Alexander J.
Journal of the Chemical Society - Perkin Transactions 1, 1998 , # 19 p. 3181 - 3206