1: With diisobutylaluminium hydride in hexane; dichloromethane
T=-78°C; 1.5 h;
2: With hydrogenchloride; water in hexane; dichloromethane
T=-78 - 20°C;
参考文献
Coldham, Iain; Jana, Samaresh; Watson, Luke; Martin, Nathaniel G.
Organic and Biomolecular Chemistry, 2009 , vol. 7, # 8 p. 1674 - 1679
lithium diisopropyl amide in tetrahydrofuran
T=-20 - 0°C;
参考文献
Miller, John F.; Furfine, Eric S.; Hanlon, Mary H.; Hazen, Richard J.; Ray, John A.; Robinson, Laurence; Samano, Vicente; Spaltenstein, Andrew
Bioorganic and Medicinal Chemistry Letters, 2004 , vol. 14, # 4 p. 959 - 963
