N-羟基邻苯二甲酰亚胺合成路线 （共 297 条）
参考文献
Kuenhle, Adolf; Duda, Mark; Jost, Carsten; Fries, Guido; Kirchhoff, Jochen; Schiffer, Thomas
Patent: US2003/176733 A1, 2003 ;
反应条件
pyridine; 4 A molecular sieve; copper(l) chloride in 1,2-dichloro-ethane T=20°C; 48 h;
参考文献
Petrassi; Sharpless; Kelly
Organic letters, 2001 , vol. 3, # 1 p. 139 - 142
反应条件
sodium acetate in N,N-dimethyl-formamide T=80°C; 14 h; Inert atmosphere;
参考文献
Canham, Stephen M.; France, David J.; Overman, Larry E.
Journal of Organic Chemistry, 2013 , vol. 78, # 1 p. 9 - 34
反应条件
sodium acetate in N,N-dimethyl-formamide T=80°C; 16 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Sebesta, David P.; O'Rourke, Sarah S.; Martinez, Rogelio L.; Pieken, Wolfgang A.; McGee, Danny P. C.
Tetrahedron, 1996 , vol. 52, # 46 p. 14385 - 14402
反应条件
1: 2-hydroxy-1,3-isoindolinedione With sodium hydride in N,N-dimethyl-formamide T=0°C; 0.25 h; 2: chloromethyl methyl sulfide in N,N-dimethyl-formamide T=60°C; 0.5 h;
参考文献
Yamashita, Tohru; Kawai, Nobutaka; Tokuyama, Hidetoshi; Fukuyama, Tohru
Journal of the American Chemical Society, 2005 , vol. 127, # 43 p. 15038 - 15039
反应条件
sodium hydroxide; sodium chloride in acetonitrile T=30°C; ΔH*, ΔS*; var. conc. NaCl, org. solvents, and temp.; Rate constantThermodynamic data;
参考文献
Khan, M. Niyaz
Journal of Physical Organic Chemistry, 1994 , vol. 7, # 8 p. 412 - 419
参考文献
Lassar-Cohn
Justus Liebigs Annalen der Chemie, 1880 , vol. 205, p. 295
反应条件
1: 2-hydroxy-1,3-isoindolinedione With sodium hydride in N,N-dimethyl-formamide T=0°C; 0.166667 h; Inert atmosphere; 2: monobromoacetic acid in N,N-dimethyl-formamide T=0 - 20°C; Inert atmosphere;
参考文献
Journal of the American Chemical Society, , vol. 133, # 19 p. 7469 - 7475
反应条件
1: potassium carbonate / 1-methyl-pyrrolidin-2-one / 20 - 50 °C / Inert atmosphere 2: trifluoroacetic acid / dichloromethane / 1.33 h / 0 °C View Scheme
反应条件
in acetic acid T=25°C; KineticsEquilibrium constant; Further Variations:Solvents;
参考文献
Cai, Yang; Koshino, Nobuyoshi; Saha, Basudeb; Espenson, James H.
Journal of Organic Chemistry, 2005 , vol. 70, # 1 p. 238 - 243
