N-羟基邻苯二甲酰亚胺合成路线 （共 297 条）
参考文献
Ranadive, V. B.; Khadilkar, B. M.; Samant, S. D.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1994 , vol. 33, p. 1175 - 1177
反应条件
1: acetonitrile / 4 h / 20 °C / |Schlenk technique; |Inert atmosphere
2: [iridium(III)(2-phenylpyridine)3] / acetonitrile / 24 h / 20 °C / |Sealed tube; |Irradiation
View Scheme
参考文献
Allen, Laura J.; Cabrera, Pablo J.; Lee, Melissa; Sanford, Melanie S.
Journal of the American Chemical Society, 2014 , vol. 136, # 15 p. 5607 - 5610
反应条件
1.1: 4-(N,N-dimethlyamino)pyridine; N-ethyl-N,N-diisopropylamine / tetrahydrofuran; dichloromethane / 48 h / 0 - 23 °C / Inert atmosphere
2.1: boron trifluoride diethyl etherate / dichloromethane / 0.5 h / 0 °C / Inert atmosphere
2.2: 1.5 h / 40 °C / Inert atmosphere
View Scheme
参考文献
Vo, Cam-Van T.; Mitchell, T. Andrew; Bode, Jeffrey W.
Journal of the American Chemical Society, 2011 , vol. 133, # 35 p. 14082 - 14089
反应条件
1: acetonitrile / 4 h / 20 °C / |Schlenk technique; |Inert atmosphere
2: [iridium(III)(2-phenylpyridine)3] / acetonitrile / 24 h / 20 °C / |Sealed tube; |Irradiation
View Scheme
参考文献
Allen, Laura J.; Cabrera, Pablo J.; Lee, Melissa; Sanford, Melanie S.
Journal of the American Chemical Society, 2014 , vol. 136, # 15 p. 5607 - 5610
参考文献
Ranadive, V. B.; Khadilkar, B. M.; Samant, S. D.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1994 , vol. 33, p. 1175 - 1177
反应条件
1: acetonitrile / 4 h / 20 °C / |Schlenk technique; |Inert atmosphere
2: [iridium(III)(2-phenylpyridine)3] / acetonitrile / 24 h / 20 °C / |Sealed tube; |Irradiation
View Scheme
参考文献
Allen, Laura J.; Cabrera, Pablo J.; Lee, Melissa; Sanford, Melanie S.
Journal of the American Chemical Society, 2014 , vol. 136, # 15 p. 5607 - 5610
反应条件
pyridine; 4 A molecular sieve; copper(l) chloride in 1,2-dichloro-ethane
T=20°C; 48 h;
参考文献
The Scripps Research Institute
Patent: US2006/178527 A1, 2006 ;
Location in patent: Page/Page column 7; 8; sheet 6 ;
反应条件
1: acetonitrile / 4 h / 20 °C / |Schlenk technique; |Inert atmosphere
2: [iridium(III)(2-phenylpyridine)3] / acetonitrile / 24 h / 20 °C / |Sealed tube; |Irradiation
View Scheme
参考文献
Allen, Laura J.; Cabrera, Pablo J.; Lee, Melissa; Sanford, Melanie S.
Journal of the American Chemical Society, 2014 , vol. 136, # 15 p. 5607 - 5610
反应条件
pyridine; N,N-dimethyl-formamide; phosphorochloridic acid diphenyl ester in dichloromethane
1.) 10 min, 2.) 2.5 h;
参考文献
Garcia, T.; Arrieta, A.; Palomo, C.
Synthetic Communications, 1982 , vol. 12, # 9 p. 681 - 690
参考文献
Ranadive, V. B.; Khadilkar, B. M.; Samant, S. D.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1994 , vol. 33, p. 1175 - 1177
