N-羟基邻苯二甲酰亚胺合成路线 (共 297 条)
反应条件
triethylamine in N,N-dimethyl-formamide
T=0°C; 0.25 h;
参考文献
Sheppard, Andrew; Miller, Marvin J.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1990 , # 9 p. 2519 - 2525
反应条件
potassium carbonate in N,N-dimethyl-formamide
12 h;
参考文献
Ranadive, V. B.; Khadilkar, B. M.; Samant, S. D.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1994 , vol. 33, p. 1175 - 1177
反应条件
pyridine; N,N-dimethyl-formamide; phosphorochloridic acid diphenyl ester in dichloromethane
1.) 10 min, 2.) 1.5 h;
参考文献
Garcia, T.; Arrieta, A.; Palomo, C.
Synthetic Communications, 1982 , vol. 12, # 9 p. 681 - 690
反应条件
pyridine; oxygen; (5,10,15,20-tetraphenylporphyrinato)manganese(III) chloride in acetonitrile
T=30°C; 3 h; Product distribution;
参考文献
Masui, Masaichiro; Tsuchida, Keiichi; Kimata, Yukio; Ozaki, Shigeko
Chemical and Pharmaceutical Bulletin, 1987 , vol. 35, # 7 p. 3078 - 3081
反应条件
pyridine; (5,10,15,20-tetraphenylporphyrinato)manganese(III) chloride in acetonitrile
20 h; Ambient temperature;
参考文献
Ozaki, Shigeko; Hamaguchi, Tomomi; Tsuchida, Keiichi; Kimata, Yukio; Masui, Masaichiro
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1989 , p. 951 - 956
反应条件
potassium hydroxide
1.) 1,2-dimethoxyethane, 5-10 deg C, 90 min; 2.) DMF, RT, 30 min; Yield given. Multistep reaction;
参考文献
Consonni, Piero; Favara, Duccio; Omodei-Sale, Amedeo; Bartolini, Giuseppe; Ricci, Alfredo
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1983 , p. 967 - 974
反应条件
pyridine; (5,10,15,20-tetraphenylporphyrinato)manganese(III) chloride in acetonitrile
T=30°C; Product distribution;
参考文献
Ozaki, Shigeko; Hamaguchi, Tomomi; Tsuchida, Keiichi; Kimata, Yukio; Masui, Masaichiro
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1989 , p. 951 - 956
反应条件
di-isopropyl azodicarboxylate; triphenylphosphine in tetrahydrofuran
T=0 - 4°C;
参考文献
SHIONOGI and CO., LTD.
Patent: EP1489084 A1, 2004 ;
Location in patent: Page 55 ;
反应条件
in ethyl acetate
T=70 - 72°C; 4 h;
参考文献
Il'ina, A. V.; Davidovich, Yu. A.; Rogozin, S. V.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1984 , vol. 33, p. 869 - 871
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1984 , # 4 p. 943 - 945
反应条件
1: 2-hydroxy-1,3-isoindolinedione With sodium hydroxide; Amberlite IRA-400 chloride form
2: 1,4-dibromo-butane in tetrahydrofuran
Heating;
参考文献
Dalal; Pawar; Mahulikar
Organic Preparations and Procedures International, 2007 , vol. 39, # 1 p. 81 - 85